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OTA
<br /> Sample ID EFFLUENT FLAG CITY CHEVRON
<br /> EPA METHOD 1613
<br /> Client Data Sample Data
<br /> L aboratorN Data
<br /> Name Caltest Analytical Laboratory
<br /> Project Matrix Effluent Lab Sample Date Received 10-Sep-02
<br />� � c09o1s8 22791-001
<br /> Date Collected 5-Sep-02 Sample Size 0 916 L QC Hatch No 3319 Date Extracted
<br /> 19-Sep-02
<br /> Time Collected 1310 Date Analyzed DB-5 21-Sep-02 Date Analyzed DB-225 NA
<br /> Analyte Cone (pg/L) DL' EMPCb MDL c Qualifiers Labeled Standard %R LCL-UCLd Qualifiers
<br /> 2,3,7,8-TCDD ND 2 18 0 637 IS 13C-2,3,7,8-TCDD 647 25- 164
<br /> 1,2,3,7,8-PeCDD ND 210 281 13C-1,2,3,7,8-PeCDD 689 25- 181
<br /> 1,2,3,4,7,8-HxCDD ND 395 1 75 13C-1,2,3,4,7,8-HxCDD 582 32- 141
<br /> 1,2,3,6,7,8-HxCDD ND 407 1 87 13C-1,2,3,6,7,8-HxCDD 698 28- 130
<br /> 1,2,3,7,8,9-HxCDD ND 399 271 13C-1,2,3,4,6,7,8-14pCDD 655 23- 140
<br /> 1,2,3,4,6,7,8-HpCDD ND 261 305 13C-OCDD 678 17- 157
<br /> OCDD ND 443 696 13C-2 3
<br /> ,7,8-TCDF 778 24- 169
<br /> 2,3,7,8-TCDF ND 2 18 1 03 13C-1,2,3,7,8-PeCDF 687 24- 185
<br /> 1,2,3,7,8-PeCDF ND 334 225 13C-2,3,4,7,8-PeCDF 733 21 - 178
<br /> 2,3,4,7,8-PeCDF ND 2 81 2 38 13C-1,2,3,4,7,8-HxCDF 530 26- 152
<br /> 1,2,3,4,7,8-HxCDF ND 0 725 238 13C-1,2,3,6,7,8-HxCDF 550 26- 123
<br /> 1,2,3,6,7,8-HxCDF ND 0 752 244 13C-2,3,4,6,7,8-HxCDF 602 28- 136
<br /> 2,3,4,6,7,8-HxCDF ND 0 906 306 13C-1,2,3,7,8,9-HxCDF 647 29- 147
<br /> 1,2,3,7,8,9-HxCDF ND 154 231 13C-1,2,3,4,6,7,8-HpCDF 663
<br /> 28- 143
<br /> 1,2,3,4,6,7,8-HpCDF ND 142 3 57 13C-1,2,3,4,7,8,9-HpCDF 67 1 26- 138
<br /> 1,2,3,4,7,8,9-HpCDF ND 203 3 13 13C-OCDF 682 17- 157
<br /> OCDF ND 472 617 CRS 37C1-2,3,7,8-TCDD 866 35- 197
<br /> Totals Toxic Equivalent Quotient(TEQ)Datae
<br /> Total TCDD ND 2 18 TEQ(Min) 0
<br /> Total PeCDD ND 2 10
<br /> Total HxCDD ND 400 a Sample specific estimated detection limit
<br /> Total HpCDD ND 261 b Estimated maximum possible concentration
<br /> Total TCDF ND 218 c Method detection limit
<br /> Total PeCDF ND 306 d Lower control limit-upper control limit
<br /> i
<br /> Total HxCDF ND 0 952 e TEQ based on World Health Organization Toxic Equivalent Factors(WHO-1997)
<br /> Total HpCDF ND 170
<br /> Analyst JMH Approved By William J Luksemburg 23-Sep-2002 13 41
<br /> Project 22791 Page 6 of 11
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