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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> • httn//www mccampbeli com E-mail main@mccampbell com <br /> Advanced GeoEnvtronlnental Client Prosect ID Fla:City Date Sampled 06/13/02 <br /> 837 Shaw Road Date Received 06/14/02 <br /> Stockton,CA 95215 Client Contact Tian Cuellar Date Extracted 06/14/02 <br /> Client P O Date Analyzed 06/17/02 <br /> tLEPA_analytical methods 6010 200 7 Metals by ICP* <br /> b ID Client ID Matrix Extraction° Manganese* iron's Aluminum* Phosphorus* <br /> 0206240 Effluent W Dissolved ND <br /> A29 ND 0 32 0 077 <br /> Reporting Limit unless W Dissolved 0 005 mg/L 0 005 001 002 <br /> otherwise stated,ND means <br /> not detected above the S FMC 1 0 mg/kg 30 — — <br /> reporting limit <br /> --- STLC,TCLP 0 10 mg/L 010 — <br /> *water samples are reported in mg/1.,sod and sludge samples in mglkg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in mg/L <br /> 'EPA extraction methods 1311(i'CLP),3010/3020(water,TTLC),3040(organic matnces,TTLC),3050(solids,TTLC),STLC-CA Title 22 <br /> a DISTLC extractions are performed using STLC methodology except that deionumd water is substituted for citric acid buffer as the <br /> extraction fluid l3ISTLC results are not applicable to STLC regulatory lunits <br /> reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than --2 vol % sedument, this sedunent is extracted with the liquid, in accordance with EPA <br /> . methodolo les and can si iHcantl effect re oiled metal cancxntratians, dissolved iron assumed to be equal to ferrous iron <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />