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• <br />• <br />11 U 2nd Avenue South, ##D7 Pacheco, CA 94553-5560 <br />McCampbcll Analytical Inc Telephone 925798-1620 Fax 925-798-1622 <br />httn //www mrra,nnh«11 rnm F-mo,i <br />Advanced GeoEnvlronmental, Inc <br />837 Shaw Road <br />Stockton, CA 95215 <br />Client Project ID Flag City Chevron <br />Date Sampled 06/14/02 <br />Date Received 06/18/02 <br />Client Contact Tun Cuellar <br />Date Extracted 06/21102-06/22/02 <br />Client P O <br />Date Analyzed 06121/02-06/22/02 <br />Oxygenated Volatile Organics by GC/MS* <br />Extraction Method SW5030B Analytical Method SW8260B Work Order 0206271 <br />Lab ID <br />0206271-013C <br />J 0206271-014C , <br />Client ID <br />MW13c/061402 <br />i MW13d/061402` <br />� <br />Reporting Limit for <br />Matrix <br />W <br />W <br />3 <br />DF =1 <br />DF <br />I <br />T S <br />w <br />Compound <br />Concentration <br />ug/kg <br />µgrL <br />Dusopropyl ether (DIPS) <br />ND <br />ND <br />NA <br />05 <br />Ethyl tert-butyl ether (ETBE) <br />ND <br />ND <br />NA <br />05 <br />Methyl -t -butyl ether (MTBE) <br />ND <br />ND <br />NA <br />05 <br />tent -Amyl methyl ether (TAME) <br />ND <br />ND <br />NA <br />05 <br />t -Butyl alcohol (TBA) <br />ND <br />ND <br />NA <br />50 <br />Methanol <br />ND <br />ND <br />NA <br />500 <br />Ethanol <br />ND <br />ND <br />NA <br />50 <br />1,2-Dibromoethane (EDB) <br />ND <br />ND <br />NA <br />05 <br />1,2-Dichloroethane (1,2 -DCA) <br />ND <br />ND <br />NA <br />05 <br />Surrogate Recoveries (%) <br />%SS <br />100 <br />101 <br />Comments <br />* water samples are reported in ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCLP I STLC I SPLP extracts to ug/L <br />ND means not detected above the reporting limit, NIA means surrogate not applicable to this analysis <br />(h) lighter than water immiscible sheen/product is present, (1) liquid sample that contains greater than —2 vol % sediment, 0) sample diluted due to high <br />organic content <br />DHS Certification No 1644 <br />Edward Hamilton, Lab Director <br />