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Sent 8y McCampbell Analytical, Inc , 1 925 798 4612, Jun -21-02 4 45PM, Page 18/28 <br />McCampbell Analytical Inc 130 2ud 1rn�ue South xtJ7 Pach— CA 94553-SSalI <br />I Teleplwne 923 79R-1620 Fax 925 7 s IL22 <br />i+uo rW u�v nx.tampheit Lam f -mail ma�w�+;mccamEtbell ermi <br />010 Advanced GeoEnvtronmental, Inc Client Project ID Flag City pate Sampled 06/13/02 <br />837 Shaw Road <br />Surrogate Recoveries (%) <br />9'oS5 l04 103 � 103 E03� <br />Comments <br />water samples are reported in ug/1 , sod and sludge samples in ug/kg wipes in uglwipe and all i CLP r STLC SDLP extra,ts in uVT_ <br />4D means not detected above the reporting ltrm 1, NIA means surrogate not applicable to this analysis <br />h) lighter than water immiscible sheenlprnduct is present (i) liquid sample that contains greater than --2 vol % sediment, 0) sarnplL diluted due in high <br />irganic Content <br />DHS Certification No 1644 Edward Hamilton, Lab Director <br />Date Received <br />06/14/02 <br />Stockton, CA 95215 <br />Client Contact Tim Cuellar <br />Date Extracted <br />06/16102-06/20/02 <br />Client P O <br />Date Analyzed <br />06/16/02-06/20102 <br />Oxygenated Volatile Organics by GC/MS* <br />Lxtraemun Method 5µa03011 <br />Analylical Method. SWRWIi <br />Lab ID <br />0206240-0260 <br />Work Order 020624U <br />0206240-0270 0206240-028CClient <br />ID6W-7 <br />70206240-0250 <br />— — <br />EW -8 <br />— — <br />EW -10 <br />— I _ _ — <br />Influent <br />Reporting Ltnut for <br />Matrix <br />W <br />W <br />W <br />W -- <br />Dr =t <br />DF <br />j - <br />--T- 1--- ---- <br />1-- <br />— - - - <br />1 <br />S W <br />Compound <br />Concentration <br />ug&kg Rg/L <br />Dilsopropyl ether (D(PE) <br />NO <br />ND <br />ND <br />ND <br />NA <br />U 5 <br />rthyl tcrt-butyl ether (FTSE) <br />NO <br />I ND <br />ND— <br />ND <br />N 0 j <br />Methyl -t -butyl ether (MTDr) <br />ND <br />a 17 — <br />— 9 2 <br />19 <br />NA 05 <br />ten -Amy] methyl ether (TAME) <br />ND— <br />ND f— <br />ND <br />� NTS <br />- — — - <br />NA 01 <br />� <br />— <br />(-Butyl niLohol (TBA) <br />ND <br />I ND <br />I <br />ND <br />I NO <br />NA 50 <br />Methanol <br />ND <br />ND — <br />-- <br />ND <br />I — — <br />4D <br />- — — - <br />NA 500 <br />-- — —� <br />--- � <br />— <br />!ethanol <br />ND <br />I ND � <br />ND <br />� � Nb <br />NA SD <br />t— <br />I <br />1 2-Dibromoethane (EDB) <br />ND <br />ND I <br />ND <br />ND <br />NA OS <br />1,2-Dichloruetkanc (1,2 -DCA) — <br />— ND <br />I-- ND — — <br />ND <br />I ND <br />NA 05 <br />Surrogate Recoveries (%) <br />9'oS5 l04 103 � 103 E03� <br />Comments <br />water samples are reported in ug/1 , sod and sludge samples in ug/kg wipes in uglwipe and all i CLP r STLC SDLP extra,ts in uVT_ <br />4D means not detected above the reporting ltrm 1, NIA means surrogate not applicable to this analysis <br />h) lighter than water immiscible sheenlprnduct is present (i) liquid sample that contains greater than --2 vol % sediment, 0) sarnplL diluted due in high <br />irganic Content <br />DHS Certification No 1644 Edward Hamilton, Lab Director <br />