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Sent By McCampbell Analytical, Inc 1 925 798 4612, Jul-10-01 5 35PM, Page 617 <br /> I 0 2nd M critic South,#D7 Pacheco,CA 94553--)56t) <br /> MCCAIIiIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h /Jww%v mccam hell trim E-mail main f�r mccampbeEl corn <br /> Dane Sampled 07/02/20 1 <br /> Advanced GeoEnvironrrtental Client Protect ID Flag Ctry Chevron P 0 <br /> 837 Shaw Road Date Received 07/03/2001 <br /> Stockton CA 95215 Client Contact Tim Cuellar Date Extracted 07/03/2001 <br /> Client P O Date Analyzed_07/052001 <br /> Lead* <br /> EPA andlyncal methods 6010/200 7 239 2' <br /> Lab ID Client 13 Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 71680 INFLUENT W TTLC NO MA <br /> 71681 UF€.UENT W TTLC ND N/A <br /> I <br /> S TTLC 30iVkg <br /> [irpiirtmg Limit unless otherwise <br /> stated,ND means not detei.taf above W TTF C 0 005 ma L <br /> the reporting limit <br />' -- STLC TCLP 02 mgll <br /> 'soi and sludge samples are reported in mg/kg,wipe samples in ug/wipc,and water samples and all$1 U_/SPLP,TCLP extracts in titglL <br /> -Lead is analysed using EPA method 6010 (ICP)tor srulb, Judges,SrLC &TCLP extracts and method 239 2 (AA Furnace) ror watei <br /> bampics <br /> r. DIS 1 LC extracnons are performed using STLC methodology except that deronized water is substituted for citric acid buffer as flit <br /> extra.Uun fluid DI'M C results are not applicable to STLC regulatory limits <br /> ° <br /> EPA cxtraetton methods 1311(TCLP) 3010/3020(watcr TTLC),3040(433"ganie matrices TTLC) 3050(solids TTI L),bTL( -CA Title 22 <br /> surrogate dtlulod out of range,N/A means sutrog,1c notapplicable w rhts analysts <br /> a repurting limit raised due matrix intertri,°nce <br /> i) liquid sample that contains greater than --2 vol 14 sediment, this sediment o extracted %%ah the liquid, in aecordaocn with IPA <br /> riiethodologics imd wn significantly effect reported irntal concrntrattons <br />' DHS Certification No 1644 Edward Hamilton,Lab Director <br />