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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 WCAUTBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell corn E-mail main@ mccampbell coin <br /> Advanced GeoEnvirotitnenml Client Project ID Flag City Chevron <br /> Date Sampled 06/14/02 <br /> 837 Shaw Road Date Received 06/15/01 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 06/15-06/19/01 <br /> rChent P Q Date Analyzed 06/15-06/19/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 69950 69951 69952 69953 <br /> Reporting Limit <br /> MWHD MW12A MW12B MW12C <br /> Client ID 061401 061401 061401 061401 <br /> Matra W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(RIPE) ND ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND ND so 10 <br /> Methyl tert-Butyl Ether(MTBE) ND 24 ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 1 0 <br /> tent-Butanol ND ND ND ND 25 50 <br /> IMethanol ND ND ND ND 2500 500 <br /> IEthanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> I <br /> Dibromofluoromethane 98 100 101 101 <br /> IComments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes to ug/wtpe and all TCLP 1 STLC/SPLP extracts to ug/L <br /> ND means not detected above the reporting ltrmt,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> I <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />