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110 2nd Avenue South,#D7,Pacheco,CA 945535560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 14 1 hap//www mccampbell cam E-mail matn@mccampbell corn <br /> IAdvanced GeoEnvironmental Client Project ID Flag City Chevron Date Sampled 03/09/2001 <br /> 837 Shaw Road Date Received 03/13/2001 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 03114-03/15/2001 <br /> Client P O Date Analyzed 43/14-03/1512001 <br /> 7 Oxygenated Volatile Organics By GC7W <br /> EPA method 8260 modified <br /> Lab ID 62480 62481 62482 62483 <br /> MW12C/3- MW12D/3- MW13A/3- MW13B/3- ReportingLumt <br /> Client ID 09-01 09-01 09-01 09-01 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND ND ND NO 5o 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl-tert Butyi Ether(MTBE) ND ND 2 7 ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND so to <br /> tert-Butanol ND ND ND ND 25 50 <br /> Methanol ND ND ND ND 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dtbromofluoromethane 115 115 116 117 <br /> Comments <br /> *water samples are reported to ug/L,soil and sludge samples to ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts to ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />