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' I 10 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 _ <br />' http//www niccampbell corn E-mail main@mccampbell com <br />' Advanced GeoEnvtronmental Client Project ID Flag City Chevron Date Sampled 02/02/01 <br /> 837 Shaw Road Date Received 02/06/01 <br />' Stockton, CA 952I5 CIient Contact Tin Cuellar Date Extracted 02/06/01 <br /> Client P O Date Analyzed 02/06/01 <br />' FPA analytical methods 6010/200 7,239 2+ Lead* <br /> Lab ID Client ID Matrix Extraction° Lead* %Recovery <br />' Surrogate <br /> 59512 Effluent W TTLC ND N/A <br /> I <br /> I <br /> S TTLC 3 0 mg/kg <br /> Reporting Lirrmt unless otherwise <br /> stated,ND means not detected above W TTLC 0 005 mg/L <br /> the reporting limit <br /> --- STLC,TCLP 0 2 mg/L <br /> "soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,and water samples and all STLC/SPI-P/TCLP extracts in mg/L <br /> Lead is analysed using EPA method 6010 (ICP)for soils sludges, $TLC $ TCLP extracts and method 2392 (AA Furnace) far water <br /> samples <br /> 4 DISTLC extractions are performed using STLC methodology except thatdeionized water is substituted for citnc acid buffer as the <br /> extraction fluid DISTLC results are not applicable to STLC regulatory limits <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,TTLC),3050(sohds,TTLC),STLC-CA Title 22 <br /> surrogate diluted out of range,N/A means surrogate not applicable to this analysis <br /> &reporting lirrut raised due matrix interference <br /> i) liquid sample that contains greater than —2 vol % sediment, this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations <br /> DHS Certification No 1644 Edward Hanulton,Lab Director <br />