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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 14 hqn//www mccampbell co m E-mail main@mccampbell com <br /> • <br /> Advanced GeoEnvironmental Client Project 1D Flag City Date Sampled 03127-03128/02 <br /> 837 Shaw Road Date Received 03/28/02 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 04/01/02 <br /> Client P O Date Analyzed 04/01/02 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab M 0203513-035 <br /> Client ID EFFLUENT <br /> Matrix W <br /> Reporting Limit Reporting L=t <br /> Compound Concentration* Compound Concentration* <br /> W s w s <br /> Acetone(b) ND 50 25 trans-l,3-Dichlaropropene ND 10 50 <br /> Benzene ND to 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br /> Bromochloromeihane ND 10 50 Hexachlorobutadiene ND so 25 <br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 50 <br /> Bromoform ND 10 50 Isopropylbenzene ND 10 50 <br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone(d) ND 10 so <br /> sec-Butyl benzene ND 1 0 50 Methylene Chlondetei ND 10 50 <br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone to ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone'g) ND to 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) PID 10 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 so <br /> Chloroethane ND<3 0 1 0 50 n-Propyl benzene ND 10 50 <br /> 2-Chloroethyl Vinyl Ether{`) ND 1 0 50 Styrene('`) ND 1 0 50 <br /> Chloroform ND 10 50 1,1,12-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 1 0 50 <br /> 4-Chlorotoiuene ND 10 50 Toluene(L) ND 10 50 <br /> Lhbromochloromethane ND 1 0 5 0 1,2,3-Tnehlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnehlorobenzene ND 50 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Trichloroethane ND 10 50 <br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Tnehloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 10 so <br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 .5() 1,2,3-Tnchlnropropane ND 10 50 <br /> I,1-Dichloroethane ND 1 0 50 1,2,4-Tnmethylbenzene ND to 50 <br /> 12-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene ND 10 50 <br /> i,]-Dichloroethene ND 1 0 50 Vinyl Acetate m ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chlonde(" ND 10 50 <br /> trans-i,2-Dichloroethene ND 1 0 50 Xylenes,total ND 10 1 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloro ro ane ND 10 50 Surrogate Recoveries <br /> 2,2-Dichlaropropane ND i 0 50 Dibromofluoromethane 101 <br /> I,l-Dichloropropene ND I 10 1 50 Toluene-M 97 <br /> CIS-1,3-Dichloro ene ND I 1 0 1 5 0 4-Bromofluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts to ug/L <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> (b) 2-pmpanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> Pentanone or isopropylacetone, (h) lighter than water immiscibie sheen is present, (t) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, ( ethylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene, o dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />