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McCain bell Analytical Inc I 1102nd hone SouW -16 Pacheco CA 98 1622560 <br /> p y I Telephone 925-798-1620 Fax 925-798 ]622 <br /> j Imp dwww mcc:IMPWl corn E mad mann a mccampbell com <br /> . Advanced GeoEnvironmental Client Project 1D Flag City Date Sampled 03/27/02 <br /> 837 Shaw Road Date Received 03/28/02 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 04/01102-04/05/02 <br /> Client P O Date Analyzed 04/01/02-04105/02 <br /> Nine Oxygenated Volatile Organics by GC/MS <br /> Extraction Method SW5030B AiWyncal Method SW9260B Work Order 0203513 <br /> Lab ID 0203513-041B 0203513-042B 0203513-0438 I 0203513-044B <br /> Client ID MW12A/032802 MW12B/032802 MW12C/032802 MW12D/032802 <br /> Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF I 1 1 1 S w <br /> Compound Concentration ug/kg ug/L <br /> Diisopropyl ether(DIPE) ND I ND ND ND ( NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 0 5 <br /> I <br /> Methyl-t-butyl ether(MTBE) 60 ND ND ND NA 05 <br /> I I <br /> tert-Amyl methyl ether(TAME) ND ND ND ND I NA 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 5 <br /> Methanol ND ND I ND ND i NA Soo <br /> Ethanol ND ND ND ND I NA 50 <br /> 1,2-Dibrnmoethane(EDB) ND ND ND ND NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 0 5 <br /> I ! <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 108 107 107 109 <br /> I 1 <br /> Comments <br /> E I <br /> I <br /> #water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts to ug/L <br /> ND means not detected above the reporting limit N/A means surrogate not applicable to this analysis <br /> (h)tighter than water immiscible sheen is present,(i)liquid sample that contains greater than--2 vol %sediment,0)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />