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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAN PBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mccampbell corn E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Flag City Chevron Date Sampled 01/03/02 <br /> 837 Shaw Road Date Received 01/04/02 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 01/04/02 <br /> Client P O Date Analyzed 01/04/02 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 87789 87790 <br /> Reporting Limit <br /> Client ID Influent Effluent <br /> Matrix W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND 50 10 <br /> Methyl tert-Butyl Ether(MTBE) 41 ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND 50 10 <br /> tert-Butanol ND ND 25 50 <br /> Methanol ND ND 2500 500 <br /> Ethanol ND ND 250 50 <br /> Surrogate Recoveries(°/a) <br /> Dibromofluoromcthane 106 92 <br /> Comments <br /> *water samples are reported in ug/L soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment 0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Harnilton,Lab Director <br />