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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hJW /w E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Flag City Chevron Date Sampled 11/10/9S <br /> 4005 North Wilson Way Date Received 11/12/98 <br />' Stockton,CA 95205 Client Contact Tim Cuellar Date Extracted 11/12-11/13/98 <br /> Client P O Date Analyzed 11112-11/13/98 <br />' Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 98505 <br /> I Client ID MW1/11-]0-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND<20 Ethylbenzene ND<20 <br /> Benzene NiX20 Hexachiorobutadiene ND<20 <br /> Bromobenzene ND<20 Iodomethane ND<20 <br /> Bromochloromethane ND<20 Isopropylbenzene ND<20 <br /> Bromodichloromethane ND<20 p-Isopropyl toluene ND<20 <br /> Bromoform ND<20 Methyl butyl ketone` ' ND<20 <br /> Bromomethane ND<20 Methylene Chloride" ND<20 <br />' n-Butyl benzene Nl <20 Methyl ethyl ketone" ND<20 <br /> sec-Butyl benzene ND<20 Methyl isobutyl ketone'8 ND<20 <br /> tert-Butyl benzene ND<20 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<20 Napthalene ND<20 <br /> Carbon Tetrachloride ND<20 n-Propyl benzene NDe20 <br /> Chlorobenzene ND<20 StlTene ND<20 <br /> Chloroethane ND<20 1,1,1,2-Tetrachloroethane ND<20 <br /> 2-Chloroethyl Vinyl Ether` 'STD<20 1,1 2,2-Tetrachloroethane ND<20 <br /> I Chloroform ND<20 Tetrachloroethene ND<20 <br /> Chloromethane ND<20 Toluene` ND<20 <br /> 2-Chlorotoluene ND<20 1,2,3 Tnchlorobenzene ND<20 <br /> 4-Chlorotoluene N D<20 1 2,4-Tnchlorobenzene ND<20 <br /> Dibromochloromethane ND<20 1,1,1-Tnchloroethane ND<70 <br /> 1,2-Dibromo-3-chloropropane ND<20 3,1,2-Tnchloroethane ND<20 <br /> Dibromomethane ND<20 Tnchloroethene ND<20 <br /> 1,2-Dichlorobenzene ND<20 Trichlorofluoromethane ND<20 <br /> 1,3-Dichlorobenzene ND<20 1 2 3-Tnchloropropane ND<20 <br /> 1,4-Dichlorobenzene ND<20 1,2,4-Tnmethylbenzene ND<20 <br /> Dichlorodinuoromethani. ND<20 1,3,5 Tnmethylbenzene ND<20 <br /> ],I-Dichloroethane ND<20 Vinyl Acetate m ND<20 <br /> 1,2-Dichloroethane ND<20 Vinyl Chloride'"' ND<20 <br /> 1,1-Dichloroethene ND<20 XNlenes,lotal '° ND<20 <br /> cis-1,2-Dichloroethene ND<20 <br /> trans-l,2-Dichloroethene ND<20 <br /> I 1,2-Dichioropropane ND<20 <br /> 1,3-Dichloropmpane ND<20 <br /> 2,2-1)1chl0roprop2ne ND<20 Comments reporting limit raised due to high oxygenate content <br /> 1,1-Dichloropropene ND<20 Surrogate Reco%cries(%} <br /> cis-1,3-Dichloropropene ND<20 Dibromofluoromethane 96 <br /> trans-1,3-Dichloropropene ND<20 Toluene-d8 97 <br /> Ethylene dibromide ND<20 4-Bromofluorobenzene 120 <br /> I water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,a ipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated µater samples 1 0 ug/L, vapor samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/v4pe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanonc or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton, Lab Director <br />