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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC 'Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmcgxDpbgllcmE-mail main@mccampbell corn <br /> Date Sampled 11/10/98 <br /> Advanced GeoEnvironmental Client Project ID Flag City Chevron <br /> Date Received 11/12/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Tim Cuellar Date Extracted 11/12-11/13/98 <br /> Client P O Date Analyzed 11112-11/13/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 98508 <br /> Client iD MW5/11-10-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ' ND<2 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND Iodomethane ND <br /> BTOmochloromelhane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-lsopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chloride" ND <br /> n-Butyl benzene ND Methyl ethyl ketone"I ND <br /> sec-Butyl benzene ND Al ethyl isobutyl ketone`s ND <br /> tert Butyl benzene Methyl tert Butyl Ether(MTBE)Carbon DisulfideND Napthalene ND <br /> Carbon TetrachlorideFND <br /> ND n-Propyl benzene ND <br /> Chlorobenzene ND St<rene"I ND <br /> Chloroethane ND 11,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether"` ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetraebloroethene ND <br /> Chloromethane ND Toluene` ND <br /> 2-Chlorotoluene ND 1 2 3-Tnch]orobenzene ND <br /> 4-Chlorotoluene ND 12,4-Tnchlorobenzene ND <br />' Dibromochloromethane ND 7_171-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Tnchloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br />' 1,3-Dichlorobenzene ND I2,3-Tnchloropropane ND <br /> 1,4-Dichlorobenzene ND 1 2 4-Trimethylbenzene ND <br /> Dichlorodifluoromethanc ND 1 3,5 Tnmethylbenzene ND <br />' l 1-Dichloroethane ND Vinyl Acetate ND <br /> 1,2-Dichloroethane ND Vinvl Chloride " ND <br /> 1,1-Dichloroethene ND X}lenes,total ND <br /> cis-1,2 Dichloroethene ND <br />' trans-1,2-Dichloroeihene ND <br /> 1 2-Diehl oropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments <br />' <br /> 1,1-Diehl oropropene ND Surrogate RecoN cries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 99 <br /> trans-],3-Dichloropropene ND Toluene-d8 110 <br /> Ethylene dibromide ND 4-Bromofluorobenzene 112 <br />' %%ater and vapor samples are reported in ugrL,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP!SPLP extracts to uglL <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg wipes <br /> 0 Zug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2 proparione or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheers is present, (t)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />