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I 10 Second Avenue South,##D7,Pacheco,CA 94553 <br /> 4 MCCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br /> http://www.mcc bell.com E-mail:main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 08/19/97 <br />' 1803 West March Lane, Ste A <br /> Date Received: 08/20/97 <br /> Stockton, CA 95207 Client Contact: Tim Cuellar Date Extracted: 09-/20/97 <br />' Client P.O: Date Analyzed: 08/20/97 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 79918 79920 79922 79924 <br /> Reporting Limit <br /> Client ID P1-16 P1-35 P1-45 PI-60 <br />' Matrix S S S S S w <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND ND ND ND 5.0 1.0 <br /> Ethanol ND ND ND ND 100 20 <br />' Ethyl tert-Butyl Ether(ETRE) ND ND ND ND 5.0 1.0 <br /> Methanol --- --- --- --- NIA NIA <br /> Methyl-tent Butyl Ether(MTBE) ND 140 ND ND 50 5.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> tert-Butanol ND ND ND ND 25 5.0 <br /> Surrogate Recoveries(A) <br /> Dibromofluoromethane 96 98 92 97 <br />' Toluene-d8 103 102 104 101 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/ripe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> 09 lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;6)sample diluted due to <br /> high organic content <br /> IDHS Certification No. 1644 Edward Hamilton,Lab Director <br />