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1 10 Second A\-cnue South,##D7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br /> 16 1 ,4 http:/hvn,w.anccampbell.corn E-mail main a mccampbell"com <br />' Advanced GeoEnvironmental Client Project ID: Fla Cit Chevron Date Sampled: 08/29/97 <br /> J '; Y <br /> 1803 West March Lane, Ste A Date Received: 09/05/97 <br />' Stockton, CA 95207 Client Contact: Tim Cuellar Date Extracted: 09/05/97 <br />' Client P.O: Date Analyzed: 09/05/97 <br /> Volatile Organics By GC/IMS <br /> EPA method 8260 <br /> Lab ID 80500 <br /> Client ID P3-20 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> 1 Acetone' ' ND trans-l,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide' ' ND <br /> Bromobenzene ND E-thylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodoniethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br />' sec-Butyl benzene ND Methylene Chloride'' ND <br /> tert-Butyl benzene ND Methyl ethyl kctone'E' ND <br /> Carbon Disulfide ND Methyl isobutyl ketoneND <br /> Carbon Tetrachloride ND Methyl Cert-Butyl Ether(MTBE) ND <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyi Vinyl Ether" ND Stvrene"' ND <br />' Chloroform ND 1,1.1,2-Teuachlaroerhane ND Chloromethane ND 1,1,.2,2-Teuachloroethone ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene _N D Toluene""' ND <br />' Dibromochloromethane ND 1,23-Trichlorobenzene ND <br /> 1,2-Dibromo-3-chi oropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromotnethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1.2-Trichloroethane ND <br />' 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2.3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br />' 1,2-Dichloroethane ND 13,3-Trime1hylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride"" ND <br /> trans-1,2-Dichloroethene ND Xylenes,total 'r ND <br />' 1,2-Dichhloropropane ND Comments; <br /> 1,3-Dichloropropane ND Surrogate Recoveries('%,) <br /> 2,2-Dichloropropane ND Dibromoil uoromethane 107 <br /> 1,1-Dichloropropene ND Toluene-d3 105 <br /> 71s-1,3-Dichloropropene ND 4-Br0m01luorobenzene 98 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,%vipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg,wipes 0.2ug/wipe <br /> I ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromelhane; (1) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> clhloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Z�Z/_ Ed%vard Hamilton, Lab Director <br />