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i <br /> 110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> 4 <br /> McCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br /> http://Nvww.mccampbcll.com E-mail: main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Flag City Chevron Date Sampled: 09/05/97 <br /> Date Received: 09/09/97 <br /> 1803 West March Lane, Ste A <br /> Stockton, CA 95207 Client Contact: Tint Cuellar Date Extracted: 09/09-09/10/97 <br /> I <br /> Client P.O: Date Analyzed: 09/09-09/10/97 <br /> Oxygenated Volatile Organics By GC/17S <br /> EPA method 8260 modified <br /> Lab 1D 80560 80562 80564 80567 <br /> Reporting Lirnit <br /> Client ID P4-20 P4-35 P4-45 P4/20'-25' <br /> iMatrix S S S W S w <br /> Compound Concentration* ug/kg ug/[_ <br /> Di-isopropyl Ether(DIPE) ND ND ND ND 5.0 1.0 <br /> Ethanol --- --- --- --- 100 20 <br /> .Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 5.0 1.0 <br /> Methanol --- FIND <br /> --- --- N/A NIA <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND 50 r5.tert-Amyl Methyl Ether(TAME) ND ND ND 5.0tert-Butanol ND ND ND ND 25 <br /> i Surrogate Recoveries <br /> Dibromotluoromethane 99 106 IN 92 <br /> iToluene-d8 102 101 101 106 <br /> Comments: <br /> i *water samples are reposed in ug/L,soil and sludge samples in ug/kg,wipes in ug/+Wipe and all']-CLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter that water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol. '%sediment;0)sample diluted due to <br /> high organic content <br /> i <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br /> i <br /> i <br />