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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: Work Order: <br /> 09-Jun-04 QC SummaIV Revolt 04052205 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: C:\HPCHEM\MS07\DATA\040525\04052506.0 Batch ID: MS07S9991A Analysis Date: 05/25/2004 09:26 <br /> Sample ID: MBLK MS07S9991A Units: pg/Kg Run ID:MSD_07_040525A Prep Date: 05/25/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REG Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> "- Benzene NO 5 <br /> Toluene NO 5 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene NO 5 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: C:\HPCHEM\MS07\DATA\040525\04052507.D Batch ID: MS07SS991A Analysis Date: 05/25/2004 09:49 <br /> Sample ID: LCS MS07S9991A Units: pg/Kg Run ID: MSD_07_040525A Prep Date: 05/25/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Umit) Qual <br /> Benzene 229 5 200 115 60 142 <br /> Toluene 245 5 200 122 58 143 <br /> Ethylbenzene 243 5 200 121 58 147 <br /> m,p-Xylene 249 5 200 124 57 147 <br /> o-XVlene 246 5 200 123 58 149 <br /> — Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: C:\HPCHEM\MS07\DATA\040525\04052510.D Batch ID: MS07S9991A Analysis Date: 05/25/200410:59 <br /> Sample ID: 04052204-58AMS Units: pg/Kg Run ID:MSD_07_040525A Prep Date: 05/23/2004 <br /> _ Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 230 5 200 0 115 31 152 <br /> Toluene 257 5 200 0 128 11 182 <br /> Ethylbenzene 261 5 200 0 131 30 161 <br /> m,p-Xylene 270 5 200 0 135 0 199 <br /> o-Xylene 262 5 200 0 131 0 208 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> _ File ID: C:\HPCHEM\MSOTDATA\040526\04052511.D Batch ID: MS07S9991A Analysis Date: 05/25/200411:20 <br /> Sample ID: 04052204-58AMSD Units: pg/Kg Run ID:MSD_07_040525A Prep Date: 05/23/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Umit) Qual <br /> Benzene 238 5 200 0 119 31 152 229.8 3.5(29) <br /> — Toluene 256 5 200 0 128 11 182 256.7 0.2(44) <br /> Ethylbenzene 257 5 200 0 129 30 161 261.4 1.6(29) <br /> m,p-Xylene 264 5 200 0 132 0 199 269.9 2.0(30) <br /> o-Xylene 258 5 200 0 129 0 208 262.4 1.6(30) <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />