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Lancaster <br /> . Laboratories Analysis Report <br /> New Holland Pike,PO Box 12425,Lancaster,PA 17605.2425•717-656-2300 Fax:717-656-2681•Www.laneasteriabs.com <br /> Page ] of 2 <br /> Lancaster Laboratories Sample No. WW 4024135 <br /> Collected:04/04/2003 15 :40 by KK Account Number: 10906 <br /> Submitted: 04/08/2003 09:20 ChevronTexaco <br /> Reported: 04/22/2003 at 15:23 6001 Bollinger Canyon Rd L4310 <br /> Discard: 05/23/2003 <br /> MW-6-W-030404 Grab Water San Ramon CA 94583 <br /> Facility# 90557 Job# 386843 GRD <br /> 139 S Center St-Stockton T0607700391 MW-6 <br /> SCS06 <br /> As Received <br /> CAT As Received Method Dilution <br /> No. Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 01728 TPH-GRO - Waters n.a. N.D. 50. ug/l 1 <br /> The reported concentration of TPH-GRO does not include MTBE or other <br /> gasoline constituents eluting prior to the C6 (n-hexane) TPH-GRO range <br /> start time. <br /> 05553 TPH - DRO CA LUFT (Waters) n.a. 150. 50. ug/1 1 <br /> According to the California LUFT Protocol, the quantitation for Diesel <br /> Range organics was performed by peak area comparison of the sample pattern <br /> to that of our #►2 fuel oil reference standard (between C10 and C28 normal <br /> hydrocarbons) . <br /> Site-specific MS/MSD samples were not submitted for the project. A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level. <br /> The surrogate data is outside the 4C limits. Results from the reextraction <br /> are within the limits. The hold time had expired prior to the reextraction <br /> so all results are reported from the original extract. The result from the <br /> reextraction is 110 ug/L. <br /> 01412 Methanol and Ethanol <br /> 01424 Methanol (by Direct Injection) 67-56-1 N.D. 1,000. ug/1 1 <br /> 02500 TPH Fuels by GC (Waters) <br /> 02501 Total TPH n.a. 490. 40. ug/1 1 <br /> 02508 TPH Motor Oil C16-C36 n.a. 490. 40. ug/1 1 <br /> Site-specific MS/MSD samples were not submitted for the project. A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level. <br /> 01594 BTEX + Oxygenates by 8260B <br /> 01587 Ethanol 64-17-5 N.D. 500. ug/1 1 <br /> 02010 Methyl Tertiary Butyl Ether 1634-04-4 N.D. 2. ug/1 1 <br /> 02011 di-Isopropyl ether 108-20-3 N.D. 2. ug/1 1 <br /> 02013 Ethyl t-butyl ether 637-92-3 N.D. 2. ug/l 1 <br /> 02014 t-Amyl methyl ether 994-05-8 N.D. 2. ug/l 1 <br /> 02015 t-Butyl alcohol 75-65-0 N.D. 100. ug/1 1 <br /> 05401 Benzene 71-43-2 N.D. 0.5 ug/1 1 <br /> 05402 1,2-Dichloroethane 107-06-2 N.D. 2. ug/1 1 <br /> 05407 Toluene 108-88-3 N.D. 0.5 ug/1 1 <br /> 05412 1,2-Dibromoethane 106-93-4 N.D. 2. ug/1 1 <br /> 0 5415 Ethylbenzene 100-41-4 N.D. 0.5 ug/1 1 <br /> 6310 Xylene (Total) 1330-20-7 N.D. 0.5 ug/l 1 <br /> #=Laboratory MethodDetection Limit exceeded target detection limit <br /> N.D.=Not detected at or above the Reporting Limit <br />