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I Lancaster Laboratories <br /> Where quality Is a science. <br /> Page 1 of 2 <br /> Lancaster Laboratories Sample No. WW 3832626 <br /> Collected: 06/05/2002 00:00 Account Number: 10869 <br /> Submitted: 06/08/2002 09:50 ChevronTexaco <br /> Reported: 06/20/2002 at 20:22 6001 Bollinger Canyon Rd L4310 <br /> Discard: 07/21/2002 San Ramon CA 94583 <br />' QA-T-020605 NA Water <br /> Facility# 90557 SZRC <br /> 139 S Center St-Stockton 70607700391 QA <br /> SCSQA <br /> As Received <br /> CAT As Received Method Dilution <br />' No. Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 01728 TPH-GRO - Waters n.a. N.D. 50- ug/l 1 <br /> The reported concentration of TPH-GRO does not include MTBE or other <br />' gasoline constituents eluting prior to the C6 (n-hexane} TPH-GRO range <br /> start time. <br /> A site-specific MSD sample was not submitted for the project. A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level. <br /> l <br /> 0412 Methanol and Ethanol <br /> 01414 Methanol (by Direct Injection) 67-56-1 N.D. 200. ug/l 1 <br /> t01594 BTEX + oxygenates by 8260B <br /> 01587 Ethanol 64-17-5 N.D. 50. ug/l 1 <br />' 02010 Methyl t-butyl ether 1634-04-4 N-D. 0.5 ug/l 1 <br /> 02011 di-Isopropyl ether 108-20-3 N.D. 0.5 ug/l 1 <br /> 02013 Ethyl t-butyl ether 637-92-3 N-D. 0.5 ug/l 1 <br /> 02014 t-Amyl methyl ether 994-05-8 N.D. 0.5 ug/l 1 <br />' 02015 t-Butyl alcohol 75-65-0 N.D. 5. ug/l 1 <br /> 05401 Benzene 71-43-2 0.7 0.5 ug/l 1 <br /> 05402 1,2-Dichloroethane 107-06-2 N.D. 0.5 ug/l 1 <br /> 05407 Toluene 108-68-3 4. 0.5 ug/l 1 <br /> I 05412 1,2-Dibromoethane 106-93-4 N.D. 0.5 ug/l 1 <br /> 05415 Ethylbenzene 100-41-4 0.6 0.5 ug/l 1 <br /> 06310 Xylene (Total) 1330-20-7 20. 0.5 ug/l 1 <br /> only one vial was submitted for the GC/MS volatile analysis. Due to <br /> instrumental issues, the initial analysis of the sample could not be <br /> used. The re-analysis was performed using a previously opened vial <br /> containing headspace; the data obtained from this re-analysis is <br /> reported above. <br /> State of California Lab Certification No. 2116 <br /> Laboratory Chronicle <br /> T Analysis Dilution <br /> No. Analysis Name Method Trial# Date and Time Analyst Factor <br /> Lancaster Laboratories, Inc. <br /> M E M B E R 2425 New Holland Pike <br /> PO 12425 <br /> � <br /> Lancaster,PA 17605-2425 <br /> 717-656-2300 Fax 717-656-2681 2216 Rev.9111/00 <br />