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Date October 28, 2004 <br />Quarter: 3`d Quarter, 2004 <br />• APPENDIX A <br />FIELD AND LABORATORY PROCEDURES <br />Sampling Procedures <br />Sampling equipment is thoroughly cleaned prior to the collection of each sample The sampling procedure for each <br />well includes measuring the water level and checking for the presence of separate -phase hydrocarbons (SPH), using <br />either an electronic indicator and a clear TeflonO bailer or an oil -water interface probe Wells not containing SPH <br />are purged of approximately three casing volumes of water (or to dryness) using a submersible pump, centrifugal <br />pump, gas displacement pump, or bailer The equipment and purging methods used for the current sampling event <br />are noted on the attached field data sheets During purging, temperature, pH, electrical conductivity, and dissolved <br />oxygen are monitored in order to document that these parameters are stable prior to collecting samples After <br />purging, water levels are allowed to partially recover Groundwater samples are collected using a clean disposable <br />Teflon@ bailer, placed into appropriate EPA -approved containers, labeled, logged onto chain -of -custody documents, <br />and transported on ice to a California state -certified laboratory <br />Decontamination Procedures <br />Prior to sampling each well, reels, and pumps will be decontaminated with a steam cleaner Sensitive equipment such <br />as the water level sounder are sprayed with a non -phosphate soap and deionized water solution and rinsed with <br />deionized water All water used for equipment decontamination is collected and contained in a truck -mounted water <br />tank <br />0 Laboratory Procedures <br />• <br />The groundwater samples are analyzed for the presence of GRO (gasoline range organics C4 — C 12) by EPA Method <br />8015B due to capacity issues at the laboratory, BTEX, fuel oxygenates, and volatile organic compounds using EPA <br />Method 8260B The methods of analysis for the groundwater samples are documented in the laboratory analytical <br />report The laboratory analytical report, chain -of -custody documentation, and field data sheets are presented as <br />Appendix B <br />Purge and Rinsate Water Disposal <br />Water generated during well sampling and equipment cleaning is pumped into a truck -mounted water tank The <br />water is transported to the Blaine Tech Services holding facility in Roseville, California, or in the ARCO holding <br />facility in West Sacramento, California, for temporary storage Dillard Environmental Services then transports the <br />water to the Altamont Landfill and Resource Recovery Facility in Altamont, California, for disposal <br />K XWproce%1J5 BP ARC01044931Quartefly3 QTR 04\4493 GwMR 3QO4 d" Page A-1 <br />