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CALIFORNIALABoRAToRySERVICES Environmental <br /> Chemistry <br /> Analysis Report Volatile Organics (Oxygenates) by Capillary GC/MS, EPA 8260B- Modified <br /> Client Philip Services Project No 023484517-A00 <br /> 210 W Sandbank Contact Mark Miward <br /> Columbia, I1 62236 Phone { ) <br /> Project Former Earthgrains Lab Contact James Liang <br />' Lab ID No T7027 <br /> Date Sampled 03/28/2002 Job No 847027 <br /> Date Received 04/09/2002 COC Log No 16504 <br /> Date Extracted N/A Batch No 32734 <br /> ' Date Analyzed 04/09/2002 Instrument nstruent I'D MSO4 <br /> Date Reported 04/10/2002 Analyst ID JENNDC <br /> Matrix WATER <br /> SURROGATE <br /> Surrogate <br /> Results Surr Conc Recovery Lower Spec Upper Spec <br /> Analyte CAS No (ug/L) (ug/L) (percent) (Limit.) (Limit) <br /> 1A / MW-1 <br /> Toluene-d8 N/A 45 5 50 0 91 72 125 <br /> ' 2A / MW-2 <br /> Toluene-d8 N/A 45 4 50 0 91 72 12S <br /> 3A / MW-3 <br /> Toluene-d8 N/A 45 8 50 0 92 72 125 <br /> 4A / MW-4 <br /> ' Toluene-d8 N/A 45 6 50 0 91 72 125 <br /> ANALYTICAL RESULTS <br /> Lab / Client ID Results Rep Limit Dilution <br /> Analyte CAS No (ug/L) (ug/L) (factor) <br /> 1A / MW-1 <br /> Di-isopropyl ether 108203 ND 5 0 1 0 <br /> Ethyl Tertiary Butyl Ether 637923 ND 5 0 1 0 <br /> Methyl t-butyl ether 1634044 ND 5 0 1 0 <br /> Tertiary Amyl Methyl Ether 994058 ND 5 0 1 0 <br /> Tertiary Butyl Alcohol 75650 ND 50 1 0 <br /> 2A / MW-2 <br /> Di.-isopropyl ether 108203 ND 5 0 1 0 <br /> Ethyl Tertiary Butyl Ether 637923 ND 5 0 1 0 <br /> Methyl t-butyl ether 1634044 ND 5 0 1 0 <br /> ' Tertiary Amyl Methyl Ether 994058 ND 5 0 1 0 <br /> Tertiary Butyl Alcohol 75650 ND 50 1 0 <br /> 3A / MW-3 <br /> Di-isopropyl ether 108203 ND 5 0 1 0 <br /> Ethyl Tertiary Butyl Ether 637923 ND 5 0 1 0 <br /> Methyl t-butyl ether 1634044 ND 5 0 1 0 <br /> Tertiary Amyl Methyl Ether 994058 ND 5 0 1 0 <br /> Tertiary Butyl Alcohol 75650 ND 50 1 0 <br /> 4A / MW-4 <br /> ' Di-isopropyl ether 108203 ND 5 0 1 0 <br /> Ethyl Tertiary Butyl Ether 637923 ND 5 0 1 0 <br /> Methyl t-butyl ether 1634044 ND 5 0 1 0 <br /> Tertiary Amyl Methyl Ether 994058 ND 5 0 1 0 <br /> Tertiary Butyl Alcohol 75650 ND SO 1 0 <br /> ND = Not detected at or above indicated Reporting Limit <br /> CA DOHS ELAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 800-638-7301 916-638-7301 Fax 916-638-4510 <br /> S <br />