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COLUMBIA ANALYTICAL SERVICES,INC. <br /> QA/QC Report <br /> Client: ARCO Products Company Service Request: S9700930 <br /> Protect: 21775-234 002/£0#21333 0012168 STOCKTON Date Collected: NA <br /> Sample Matrix: Water Date Received: NA <br /> Date Extracted: NA <br /> Date Analyzed: <br /> Matrix Spike Summary <br /> TPH as Gasoline <br /> Sample Name BATCH QC Units ug(L(ppb) <br /> Lab Code S9700932-00IMS Basis NA <br /> Test Notes <br /> CAS <br /> Percent <br /> Spiked Recovery <br /> Prep Analysis Spike Sample Sample Percent Acceptance Result <br /> Analyte Method Method MRL Level Result Result Recovery Limits Notes <br /> Gasoline EPA 5030 CA/LUFT 50 250 ND 250 100 75-135 <br /> MS/020597p <br /> Page 18 <br />