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COLUMBIA ANALYTICAL SERVICES, INC - <br /> QA/QC Report <br /> Client ARCO Products Companv Service Request S960329 <br /> Project 21775-234 002/#TO19350 00/#2168 STOCKTON Date Collected 2/27/96 <br /> Sample Matrix Water Date Received 2128196 <br /> Date Extracted NA <br /> Date Analvzed 318/96 <br /> Surrogate Recovery Summary <br /> BTEX and TPH as Gasoline <br /> EPA Methods 5030/8020/California DHS LUFF Method <br /> PID Detector FID Detector <br /> Pert.Lnt RCLO%ery Percent RLLo%ery <br /> Sample N,)me Lal) Code 4-Bromotluorobenzene 4 OL ix.-Ti i(luorotoiucnc <br /> MW-3(53) 59600328-001 89 105 <br /> MW-4(59) S9600328-002 92 t02 <br /> MW-5(55) S9600328-003 92 99 <br /> MW-6(45) 59600328-004 89 101 <br /> MW-7(48) S9600328-005 93 104 <br /> Method Blank S960308-MB 93 94 <br /> Batch QC S9600335-001MS 94 97 <br /> Batch QC 59600335-001 DMS 92 97 <br /> CAS Acceptance Limits 69-116 69-116 <br /> SUP 2/060104 <br /> Page 9 <br />