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brive <br /> Sequoia SSS Jarvis95037 <br /> Morgan Nllh tq 95037 <br /> 4 (40B)776-9600 <br /> IiNAnalytical www (4W)782-63M <br /> sequolalabs corn <br /> L� <br /> Blaine Tech Services(Shell) Project 440 W Charter Way <br /> 1680 Rogers Avenue Project Number 440 W Charter Way Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 10/16/00 11 52 <br /> Volatile Organic Oxygenated Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical- San Carlos <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Lin is RPD Limit Notes <br /> Batch 0090045-EPA 5030B [P/TI <br /> LCS(0090045-BS2) _ Prepared&Analyzed 09/10/00 _ <br /> Methyl tert-buty]ether 51 4 200 ug/l 500 T 103 700-130 <br /> Surrogate 12-Dichloroethane-d4 498 "T— 500 996 760-114 <br /> Surrogate Toluene-d8 508 500 102 880-110 <br /> Matrix Spike(0090045-MSI) .-----Source L009038-05 Prepared&Analyzed 09/09/00 <br /> Methyl tert-butyl ether 501 200 ug/l 500 ND 100 600-140 <br /> Surrogate 1 2-Dichloroethane-d4 -- - - ---- 512 �-_--_ " ---- 500 --_- -101 760-114---- ------_--- - - <br /> Surrogate Toluene-d8 498 500 996 88 0-I10 <br /> Matrix Spike Dup(0090045-MSD]) Source L009038-05 Prepared&Analyzed 09/09/00 <br /> Methyl ten-butyl ether 486 200 ug/I 500 ND 972 600-140 284 _ 250 - <br /> Surrogate 11-Dichloroethane-d4 - 491- -- 500 982 982 760-114----- �� <br /> Surrogate Toluene-d8 501 500 100 880110 <br /> Batch 0090050-EPA 5030B PIT <br /> Blank(0090050-BLKI) _ Prepared&Analyzed 09/10/00 <br /> Ethanol ND 1000=ug/! - - ----- ------ _�_ <br /> 1,2-Mbromoethane ND 200 " <br /> 1,2-Dichloroethane _ - Nb -_ 200 " <br /> - - <br /> Di-isopropyl ether ND 200 <br /> Ethyl tert-butyl ether _ NU - ---�200- -- �- --- - -- - - --- - - -- - - - - - - �- <br /> Methyl tert-butyl ether ND 200 " <br /> Tert-amyl methyl ether ND 200 " <br /> Ten-butyl alcohol ND 100 " <br /> Surrogate 11-Dichloroethane-d4 476 500 952 760-114 <br /> Surrogate Toluene-d8 490 500 980 880-110 <br /> Sequoia Analytical-Morgan Hill The results in this report apply to the samples analyzed in accordance with the c <br /> custody document This analytical report must be reproduced in its entirety <br /> Page 25 of 28 <br />