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885 Jarvis Drive <br /> �} Sequoia Morgan 95037 <br /> (400 778)776-9600 <br /> FAX(408)782-6308 <br /> Analytical wwwsequeialabscom <br /> Blaine Tech Services(Shell) Project 440 W Charter Way <br /> 1680 Rogers Avenue Project Number 440 W Charter Way Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 10/16/00 1 1 52 <br /> Volatile Organic Oxygenated Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical - San Carlos <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limtts RPD Limit Notes <br /> Batch 0090050-EPA 5030B [P/T <br /> Blank(0090050-BLK2) _ Prepared&Analyzed 09/11/00 <br /> Ethanol ND 1000 ugA <br /> 1,2-Dibromoethane ND 200 " <br /> 1,2-Dichloroethane ND 200 " <br /> a-isopropyl ether ND 200 " <br /> Ethyl tent-bury]ether <br /> ND 200 " <br /> Methyl tert-butyl ether ND 200 " <br /> Tert-amyl methyl ether ND 200 <br /> Tert-butyl alcohol ND 100 _ -----___—� _ -- ---_ ---- -- - <br /> Surrogate 11-Dtchloroethane-d4 498 500 996 760-114 <br /> Surrogate Toluene-d8 481 500 961 880-110 <br /> ift(00900_50-BSI) _______-___- Prepared&Anatyzed 09/10/00 <br /> thyl ter(-butyl ether 514 200 ugll _-�50 0 —-`103 700-130 f—_ --------- <br /> Surrogate <br /> -- <br /> Surrogate 11-Dtchloroethane d4 498 500 996 760-114 <br /> Surrogate Toluene-d8 508 500 102 880-110 <br /> LCS 0090_050-BS2 __ _ Prepared&Analy?ed 09/11/00 _-- <br /> Methyl tert-butyl ether 480 200 ugA 500 _ 960 700-130 <br /> Surrogate 1 1-Dtchloroethane d4 491 500 982 760-114 <br /> Surrogate Toluene-d8 484 500 968 880-110 <br /> Matrix Spike(0090050-MSI)— _ —_— Source L009039-01 _ Prepared&Analyzed 09/10/00 _��— <br /> Methyl tert-butyl ether 483 200_ ugA _ 500 — ND966 600-140 <br /> Surrogate 1 2-Dichloroethane-d4 — 480 500 960 760-114 <br /> Surrogate Toluene-d8 500 500 100 880-110 <br /> Matnx Spike Dup(0090050-MSDI) Source L009039-01 Prepared&Analyzed 09/10/00 <br /> Methyl tent-butyl ether 53 3 200 ugA 500 _ ND 107 600-140 102 Y_ 250 <br /> Surrogate 11-Dtchloroethane-d4 _ 506 500 101 760-114 <br /> Surrogate Toluene-d8 493 500 986 880-110 <br /> nota Analytical-Morgan Hill The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document Dus analytical report must be reproduced in its entirety <br /> Page 26 of 28 <br />