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COLUMBIA ANALYTICAL SERVICES,INC <br /> QAIQC Report <br /> Client Equiva Services Service Request 59902059 <br /> Project SAP 121258/lncident 88870583 Date Collected NA <br /> Sample Matrix Soil Date Received NA <br /> Date Prepared 7114199 <br /> Date Analvzed 7115199 <br /> Matrix Sptke/Duplicate Matrix Spike Summary <br /> Metals <br /> Sample Name BATCH QC Units mglL(ppm) <br /> Lab Code 59902085-0022MS, 59902085-0022DMS Basis NA <br /> Test Notes <br /> Percent Recovery <br /> CAS Relative <br /> Prep Analysis Spike Level Sample Spike Result Acceptance Percent Result <br /> Analyte Method Method MRL MS DMS Result MS DMS MS DMS Limits Difference Nates <br /> Lead mg/L(ppm) 6010A 05 050 050 ND 034 035 68 70 75-125 3 A <br /> A Outside of acceptance limits Because LCS results were acceptable,no further corrective action <br /> was taken <br /> Approved By Date <br /> DM&020597p <br />