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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client Equiva Services Service Request K9904880� <br /> Project. [nLident# 88870583/SAP#121258 Date Colles-ted 6/29/99 <br /> Sample Matrix Soil Date Received 6/30/99 <br /> Date TCLP Performed 7/27/99 <br /> Date Extracted 7/28/99 <br /> Date Analyzed. 7/30/99 <br /> Toxicity Characteristic Leachmg Procedure(TCLP) <br /> EPA Method I311 <br /> Semivolatrle Organic Compounds <br /> Sample Name SP-14A.13 COMP Units mg/1.(ppm) <br /> Lab Code K9904880-050 Basis NA <br /> Test Notes <br /> Prep Analysis Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Pyndine EPA 3510M 82700 025 1 5 ND <br /> 2-Methylphenol EPA 3510M 82700 01 1 200 ND <br /> Hexaehloroethane EPA 3510M 8270C 0 1 1 3 ND <br /> 3-and 4-Methylphenol Coeluti EPA 351 OM 8270C 0 1 1 200 ND <br /> Nitrobenzene EPA 3510M 8270C 0 1 1 2 ND <br /> HexachlorobutadienL CPA 3510M 8270C 01 1 0 5 ND <br /> 2,4,6-Tnehlorophenol EPA 3510M 8270C 01 1 2 ND <br /> 2,4 5-Tnchlorophtnol EPA 351OM 8270C 0 1 1 400 ND <br /> 2,4-Dinitrotoluene EPA 3510M 8270C 0 1 1 0 13 ND <br /> Hexachlorobenzem. EPA 3510M 8270C 0 1 1 0 13 ND <br /> Pentachlorophenol(PCP) EPA 3510M 8270C 025 1 100 ND <br /> * From 40 CFR Part 261,et al and Federal Register,March 29, 1990 and dune 29, 1990 <br /> Approved By Date <br /> 9- '-r'55 <br /> TCLP 1 S22I052593 <br /> Page 19 <br />