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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client Equcva Services Service Request K9904880• <br /> Protect Indent# 88870583/SAP#121258 Date Collected 6/29199 <br /> Sample Matrix Soil Date Received 6130199 <br /> Date TCLP Performed 7/27199 <br /> Date Extracted 7128199 <br /> Date Analyzed 7130199 <br /> Toxicity Characteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Semivolatile Organic Compounds <br /> Sample Name SP-16AB COMP Units mg/L(ppm) <br /> Lab Code K9904880-052 Bans NA <br /> Test Notes <br /> Prep Analysis Dilution Regulatory Result <br /> Analyte Method Method MRI, Factor Limit* Result Notes <br /> Pyndme EPA 3510M 8270C 025 1 5 ND <br /> 2-Methylphenol EPA 3510M 82700 0 1 1 200 ND <br /> Hexaehloroethane EPA 3510M 8270C 0 1 1 3 ND <br /> 3-and 4-Methylphenol Coeluti EPA 3510M 8270C 0 1 1 200 ND <br /> Nitrobenzene EPA 3510M 8270C 0 1 1 2 ND <br /> Herachlorobutadiem. EPA 3510M 8270C 0 1 1 05 ND <br /> 2,4,6-Trichlorophenol EPA 3510M 8270C 0 1 1 2 ND <br /> 2,4,5-Trichlorophenol EPA 3510M 8270C 0 1 1 400 ND <br /> 2,4-Dinitrotolucm EPA 3510M 8270C 0 1 1 013 ND <br /> Hexachlorobenzem EPA 3310M 8270C 01 1 013 ND <br /> Pentachlorophenol(PCP) EPA 3510M 8270C 025 1 100 ND <br /> " From 40 CFR Part 261,eta] and Federal Register,March 29, 1990 and Jun 29, 1990 <br /> Approved By V fz Date <br /> -e7 ! <br /> TCLPis2v052595 <br /> Page 21 <br />