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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client Equlva Servl+,es Service Request K990488 <br /> Protect- Incident 88870583/SAP#121258 Date Collected 6/29/99 <br /> Sample Matrix- Soil Date Received 6/30/99 <br /> Date TCLP Performed 7/27/99 <br /> Date Extracted 7/28/99 <br /> Date Analyzed- 7/30/99 <br /> Toxicity Characteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Semivolatile Organic Compounds <br /> Sample Name SP-18AB COMP Units mg/L(ppm) <br /> Lab Code K9904880-054 Basis NA <br /> Test Notes <br /> Prep Analysts Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Pyndme EPA 3510M 8270C 025 1 5 ND <br /> 2-Methylphenol EPA 3510M 9270C 01 1 200 ND <br /> Hexaehloroethane EPA 3510M 82700 01 1 3 ND <br /> 3-and 4-Methylphenol Coelutl EPA 3510M 82700 01 1 200 ND <br /> Nitrobenzene EPA 3510M 8270C 01 1 2 ND <br /> Hexaehlorobutadlene EPA 3510M 8270C 01 1 05 ND <br /> 2,4,6-Trichlorophenol EPA 3510M 8270C 01 1 2 ND <br /> 2,4,5-Tnehlorophenol EPA 3510M 8270C 01 1 400 ND <br /> 2,4-Dmitrotoluene EPA 3510M 8270C 0 1 1 0 13 ND <br /> Hexachlorobenzene EPA 3510M 8270C 0 1 1 0 13 ND <br /> Pentachlorophenol(PCP) EPA 3510M 8270C 025 1 100 ND <br /> * From 40 CFR Part 261,et al and Federal Register,March 29, 1990 and June 29, 1990 <br /> Approved By Date D '�"(-5 S • <br /> TCLP l S22l052595 <br /> Page 23 <br />