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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> Client Equiva Services Service Request K9904880 <br /> Protect- Inudent# 88870583/SAP#121258 Date Collected 6/29/99 <br /> Sample Matrix Soil Datt Received 6/30/99 <br /> Date TCLP Performed 7/27/99 <br /> Date Extracted 7/28/99 <br /> Date Analyzed 7/29/99 <br /> Matrix Spike Summary <br /> Toxicity Ch iractenstic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Semivolahle Organic Compounds <br /> Sample Name SP-18AB COMP Units mg/L(ppm) <br /> Lab Code K9904880-054MS Basis NA <br /> Test Notes <br /> Spiked <br /> Prep Analysis Spike Sample Sample Percent Result <br /> Analyte Method Method NIRL Level Result Result Recovery Notes <br /> Pyndme EPA 3510M 8270C 025 050 ND 020 40 <br /> 2-Methylphenol EPA 3510M 8270C 0 1 05 ND 05 100 <br /> Hexachloroethane EPA 3510M 8270C 0 1 05 ND 05 100 <br /> 3-and 4-Methylphenol Coelut EPA 35 I0M 8270C 0 1 10 ND 08 80 <br /> Nitrobenzene EPA 3510M 8270C 0 1 05 ND 05 100 <br /> Hexachlorobutadiene EPA 3510M 8270C 0 1 05 ND 05 100 <br /> 2,4,6-Tnohlorophenol EPA 3510M 8270C 0 1 0 5 ND 05 100 <br /> 2 4,5-Trichlorophenol EPA 3510M 8270C 0 1 05 ND 05 100 <br /> 2,4-Dmitrotoluene EPA 3510M 8270C 0 10 050 ND 050 100 <br /> Hexachlorobenzene EPA 3510M 82700 0 10 050 ND 0 50 100 <br /> Pentachlorophenol(PCP) EPA 3510M 82700 0 25 0 50-ND-0 35 70 <br /> o t <br /> Approved By Date <br /> TCLPMS/052393 <br /> Page 27 <br />