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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client. Equlva Services Service Request. K9904980� <br /> Project: IDUdent# 88870583/SAP#121258 Date Collected- 6/29/99 <br /> Sample Matrix Soil Date Received 6130/99 <br /> Date TCLP Performed 7/28199 <br /> Date Extracted: NA <br /> Date Analyzed. 7/29/99 <br /> Toxicity Charactenstic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Volatile Organic Compounds <br /> Sample Name SP-15AB COMP Units mg/L(ppm) <br /> Lab Code K9904880-051 Basis NA <br /> Test Notes <br /> Prep Analysis Dilution Regulatory Result <br /> Analyte Method Method MRF. Factor Limit* Result Notes <br /> Benzene EPA 1311 8260B 0 2 1 05 ND <br /> Carbon Tetrachloride EPA 1311 8260B 02 1 0 5 ND <br /> Chlorobenzene EPA 1311 8260B 0 2 1 100 ND <br /> Chloroform EPA 1311 8260B 0 2 1 6 ND <br /> 1,4-Dichlorobenzene EPA 1311 8260B 0 2 1 7 5 ND <br /> 1,2-Dlchloroethane(EDC) EPA 1311 8260B 0 2 1 0 5 ND <br /> 1,1-Dtehloroethene EPA 1311 8260B 0 2 1 0 7 ND <br /> 2-Butanone(MEK) EPA 1311 8260B 10 1 200 ND <br /> Tetrachloroethene(PCE) EPA 1311 8260B 02 1 0 7 ND <br /> Trichloroethene(TCE) EPA 1311 8260B 0 2 1 0 5 ND <br /> Vinyl Chloride EPA 1311 8260B 0 2 1 0 2 ND <br /> * From 40 CFR Part 261,et al,and Federal Register,March 29, 1990 and June 29, 1990 <br /> Approved By Date 0 f '! 1 • <br /> TCLP l S22/052595 <br /> Page 33 <br />