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COLUMBIA ANALYTICAL SERVICES,INC <br /> QAIQC Report <br /> Client Equiva ServtLCS Service Request: K9904880 <br /> Project: Incident# 88870583/SAP#121258 Date Collected: 6/29199 <br /> Sample Matrix Soil Date Received: 6/30/99 <br /> Date TCLP Performed: 7/27-28/99 <br /> Date Extracted NA <br /> Date Analyzed 7/29/99 <br /> Surrogate Recovery Summary <br /> Toxicity Characteristic Leaching Procedure (TCLP) <br /> EPA Method 1311 <br /> Volatile Organic Compounds <br /> Prep Method EPA 1311 Units PERCENT <br /> Analysis Method 8260B Basis NA <br /> Test P e r c e n t R e c o v e r y <br /> Sample Name Lab Code Notes Dibromofluoromethane Toluene-ds 4-Bromofluorobenzene <br /> SP-10AB COMP K9904880-046 106 100 92 <br /> SPA lAB COMP K9904880-047 100 98 96 <br /> SP-12AB COMP K9904880-048 106 100 92 <br /> SP-13AB COMP K9904880-049 109 100 93 <br /> SP-14AB COMP K9904880-050 108 100 92 <br /> SP-I SAB COMP K9904890-051 106 99 92 <br /> SP-16AB COMP K9904880-052 _ 101 97 96 <br /> SP-17AB COMP K9904880-053 100 98 96 • <br /> SP-18AB COMP K9904880-054 98 97 95 <br /> SP-1AB COMP K9904880-037MS 99 98 100 <br /> Lab Control Sample K990729-LCS 99 97 104 <br /> Method Blank K990727-MB 100 97 97 <br /> Method Blank K990728-MB 107 98 94 <br /> CAS Acceptance Linuts 86-113 91-108 83-112 <br /> Approved By Date <br /> SUR-VO52395 <br /> Page 39 <br />