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VOC ANALYTICOGLENDALE • OAGE 1 QC REPORT FOR 9705352 DATE PRINTED- 04 JON 1997 AQUEOUS SAMPLES ------ METHOD BLANK ------ --------------- LAB CONTROL -------------- ---------------- MATRIX QC ---------------- LCS LCSD RPD RPD MS MSD RPD RPD UNITS RESULT ROL FLG %RIC FLG %REC FLG LCL UCL RPD UCL FLG %REC FLG °eREC FLG ECL UCL RPD UCL FLG Batch GAS*975081 Method 8015M TX - Modified 8015 Benzene ug/L 0 0 5 - 98 - - - 76 155 - - - 93 - 97 - 70 153 4 25 - Toluene ug/L 0 0 5 - 101 - - - 72 121 - - - 82 - 85 - 69 119 3 25 - Ethylbenzene ug/L 0 0 5 - 104 - - - 72 115 - - - 95 - 96 - 68 116 1 25 - Methyl-tert-butylether ugh 0 30 - 102 - - - 62 159 - - - 105 - 111 - 80 176 5 25 - Total Xylene Isomers ug/L 0 0 5 - 106 - - - 68 115 - - - 82 - 84 - 61 118 2 25 - TPH (Gasoline Range) ug/L 0 50 - 91 - - - 85 120 - - - 95 - 95 - 78 124 1 25 - I [a,a,a-Trifluorotoluene] Percent 134 - Q 97 - - - 85 118 - - - 96 - 95 - 85 118 - - - Batch GAS*976051 Method. 8015H TX - Modified 8015 Benzene ug/L 0 0 5 - 106 - 103 - 76 155 3 - - - - - - - - - - Toluene ug/L 0 0 5 - 109 - 107 - 72 121 2 - - - - - - - - - - - Ethylbenzene ug/L 0 0 5 - 109 - 104 - 72 115 4 - - - - - - - - - - Methyl-tert-butylether ug/L 0 30 - 86 - 115 - 62 159 29 - - - - - - - - - - Total Xylene Isomers ug/L 0 0 5 - 110 - 106 - 68 115 4 - - - - - - - - - - - TPH (Gasoline Range) ug/L 0 50 - 99 - 104 - 85 120 4 - - - - - - - - - - - [a,a,a-Trifluorotoluene] Percent 106 - - 115 - 103 - 85 118 - - - 126 Q 128 Q 85 118 - - - Batch- GAS*976052 Method- 8015M TX - Modified 8015 Benzene ug/L 0 0 5 - 101 - 100 - 76 155 1 - - 108 - 99 - 70 153 8 25 - Toluene ug/L 0 0 5 - 106 - 101 - 72 121 4 - - 92 - 92 - 69 119 1 25 - Ethylbenzene ug/L 0 0 5 - 103 - 99 - 72 115 5 - - 94 - 92 - 68 116 1 25 - Methyl-tert-butylether ug/L 0 30 - 112 - 107 - 62 159 4 - - 134 - 131 - 80 176 2 25 - Total Xylene Isomers ug/L 0 0 5 - 107 - 101 - 68 115 6 - - 80 - 78 - 61 118 2 25 - TPH (Gasoline Range) ug/L 0 50 - 99 - 100 - 85 120 1 - - 95 - 95 - 78 124 1 25 - [a,a,a-Trifluorotoluene] Percent 105 - - 95 - 99 - 85 118 - - - 131 Q 129 Q 85 118 - - - Batch• GAS*977061 Method. 8015M TX - Modified 8015 Benzene ug/L 0 0 5 - 97 - - - 76 155 - - - 115 - 113 - 70 153 2 25 - Toluene ug/L 0 12 0 5 - 98 - - - 72 121 - - - 79 - 78 - 69 119 0 25 - Ethylbenzene ug/L 0 0 5 - 101 - - - 72 115 - - - 90 - 89 - 68 116 1 25 - Methyl-tert-butylether ug/L 0 30 - 110 - - - 62 159 - - - 98 - 103 - 80 176 5 25 - Total Xylene Isomers ug/L 0.24 0 5 - 102 - - - 68 115 - - - 75 - 76 - 61 118 0 25 - TPH (Gasoline Range) ug/L 0 50 - 103 - - - 85 120 - - - 94 - 95 - 78 124 1 25 - [a,a,a-Trifluorotoluene] Percent 95 - - 96 - - - 85 118 - - - 97 - 96 - 85 118 - - -