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BC ANALYTICAL • ORDER QC REPORT FOR G9608573 ITE REPORTED 09/04/96 Page 1 MATRIX QC PRECISION (DUPLICATE SPIKES) BATCH QC REPORT SAMPLE DATE BATCH MS MSD RELATIVE aRAMETER NUMBER ANALYZED NUMBER RESULT RESULT UNIT % DIFF GRO 9608445*6 Date Analyzed 08.27.96 966130 08/27/96 08/27/96 Date NIA Benzene 08.27 96 966130 15.9 15.9 ug/L 0 Toluene 08.27 96 966130 89.6 89.2 ug/L 0 Ethylbenzene 08.27.96 966130 19.2 19. 1 ug/L 1 Total Xylene Isomers 08.27.96 966130 108 108 ug/L 0 TPH (Gasoline Range) 08.27.96 966130 1090 1100 ug/L 1 a,a,a-Trifluorotoluene Rep. 08.27 96 966130 52.6 52 7 ug/L 0 a,a,a-Trifluorotoluene Th. 08.27 96 966130 50.0 50.0 ug/L 0 BTEX (8020)/GRO 9608450*1 Date Analyzed 08.27.96 964129 08/27/96 08/27/96 Date N/A Benzene 08.27.96 964129 22.4 22.5 ug/L 0 Toluene 08.27.96 964129 89. 1 90.5 ug/L 2 Ethylbenzene 08.27.96 964129 19 1 19 1 ug/L 0 Total Xylene Isomers 08.27 96 964129 100 102 ug/L 2 lo (Gasoline Range) 08.27.96 964129 1120 1150 ugh 3 ,a-Trifluorotoluene Rep. 08.27.96 964129 59.9 62 5 ug/L 4 a,a,a-Trifluorotoluene Th. 08.27.96 964129 50.0 50.0 ug/L 0 MTBE 9608451*1 Date Analyzed 08.27.96 964129 08/27/96 08/27/96 Date N/A Methyl-tert-butylether 08.27 96 964129 164 165 ug/L i a,a,a-Trifluorotoluene Rep. 08.27.96 964129 59.9 62 5 ugh 4 a,a,a-Trifluorotoluene Th. 08.27.96 964129 50.0 50.0 ug/L 0 GRO 9608573' 6 Date Analyzed 08.28.96 964130 08/28/96 08/28/96 Date N/A Benzene 08.28.96 964130 21.7 22.1 ug/L 2 Toluene 08.28.96 964130 89.2 91 2 ug/L 2 Ethylbenzene 08.28 96 964130 18.4 18.9 ug/L 3 Methyl-tert-butylether 08.28.96 964130 175 180 ug/L 3 Total Xylene Isomers 08.28.96 964130 101 103 ug/L 2 TPH (Gasoline Range) 08.28.96 964130 1100 1120 ug/L 2 a,a,a-Trifluorotoluene Rep 08.28.96 964130 61 .9 61.4 ug/L 1 a,a,a-Trifluorotoluene Th. 08.28 96 964130 50.0 50 0 ug/L 0