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LancasterRe orf <br /> Laboratories Analysis p <br /> 5 New Holland Pike PO Box 12425 Lancasler PA 17605-2425•717 656 2300 Fax 717 656 2681•WWW 1811c85tEfIabS GOBI <br /> Page 2 of 7 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 864689 <br /> Reported 02/23/04 at 04 21 PM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL Units %REC 3REC Limits RPD RPD Max <br /> 3,31-Dxchlorobenzidxne N D 1 ug/1 89 30-108 <br /> bis(2-Ethylhexyl)phthalate N D 2 ug/1 82 62-126 <br /> Di-n-octylphthalate N D 2 u9/1 72 62-118 <br /> Benzo(b)fluoranthene N D 1 ug/l 80 71-116 <br /> Benzo(k)fluoranthene N D 1 ug/1 77 72-116 <br /> Benzo(a)pyrene N D 1 ug/1 80 74-116 <br /> Indeno(1,2,3-cd)pyrene N D 1 ug/1 85 70-120 <br /> Dibenz(a,h)anthracene N D I ug/l 90 76-128 <br /> Benzo(g,h,i)perylene N D I ug/l 88 70-121 <br /> 2-Methylphenol N D 1 ug/1 70 52_105 <br /> 4-Methylphenol N D 2 ug/1 69 54-100 <br /> Benzyl alcohol N D 5 ug/1 82 <br /> Benzoic acid N D 6 ug/1 84* 6-73 <br /> Batch number 040470024A Sample number(S) 4216136 <br /> TPH - DRO CA LUFT (Waters) N D 50 ug/1 86 89 61-126 3 20 <br /> Batch number 04047112601A �SaDmple numb0er4(0) 4216136 <br /> mg/l 93 54-133 <br /> TRPH 418 1 <br /> Batch number 04047A16A Sample number(s) 4216135 <br /> -GRO - Waters N D 50 ug/1 98 112 7D-130 13 30 <br /> Isch number 040481648001 Sample numbOr0s) 4 2 6137g/I 101 97-111 <br /> Cadmium 95-112 <br /> Chromium N D 0 0022 mg/l 100 93-110 <br /> Lead N D 0 0093 mg/1 102 g3-110 <br /> Nickel N D 0 0038 mg/1 101 <br /> Zinc N D 0 0041 mg/1 101 94-112 <br /> Batch number 04049A07A sample number(s) 4216136 70-13D <br /> TPH-GRO - Waters N D 50 ug/l 90 <br /> Batch number 04049A07B Sample number(s) 4216138-4216139 70_13D <br /> TPH-GRO - Waters N D 50 ug/l 96 <br /> Batch number N040432AC Sample number(s) 4216136 77 127 <br /> Methyl Tertiary Butyl Ether N D 0 5 ug/l 103 69-136 <br /> Chloromethane N D 1 ug/1 106 71-129 <br /> vinyl Chloride N D 1 ug/l 104 46-138 <br /> Bromomethane N D 1 ug/l 99 101 59-133 <br /> Chloroethane N D 1 ug/ 59-137 <br /> Trichlorofluoromethane N D 2 ug/1l 95 79_130 <br /> 1,1-Dichloroethene N D 0 8 ug/1 95 <br /> Methylene Chloride N D 2 ug/1 980-128 <br /> trans-1,2-Dichloroethene N D 0 8 ug/1 955 81-124 <br /> 1,1-Dxchloroethane N D 1 ug/1 98 83-127 <br /> cis-1,2-Dichloroethene N D 0 8 ug/1 97 84-117 <br /> Chloroform N D 0 8 u9/1 98 86-124 <br /> 1,1,1-Trichloroethane N D 0 8 ug/1 96 83-127 <br /> Carbon Tetrachloride N D 1 ug/1 95 77-130 <br /> Benzene N D 0 5 ug/1 100 85-117 <br /> 1,2-Dachlaroethane N D 0 5 ug/l 96 77-132 <br /> Trichloroethene N D 1 ug/ 96 87-13'7 <br /> 1,2-Dichloropropane N D 1 ug/1 99 83-121 <br /> Bromodichloromethane N D 1 ug/l 96 <br /> *- Outside of specification <br /> } The result for one or both determinations was less than five times the LOQ <br /> The background result was more than four times the spike added <br />