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Sequoia 680 Chesapeake Drive Redwood Ciry, CA 94063 (415) 364 9600 FAX (415)364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX (916)921 0100 <br /> Blaine Tech Services, Inc Client Project ID Chevron 9-2033 /961125-All <br /> 985 Timothy Drive Matrix Liquid <br /> San Jose, CA 95133 <br /> Attention Jim Keller Work Order# 9611 H98-01 Reported Dec 11, 1996 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte: Diesel <br /> QC Batch#: GC12069WHBPEXA <br /> Anally. Method' EPA S015M <br /> Prep. Method EPA 3510 <br /> Analyst B Sullivan <br /> MS/MSD # 9611139502 <br /> Sample Cone 4600 <br /> Prepared Date 12/6/96 <br /> Analyzed Date 12/9/96 <br /> Instrument 1 D # GCHP5 <br /> Cone Spiked, 1000pg/L <br /> Result- <br /> MS % Recovery* <br /> • Dup Result: <br /> MSD %Recov : <br /> RPD <br /> RPD Limit- <br /> LCS #' BLK120696 <br /> Prepared Date: 12/6/96 <br /> Analyzed Date: 12/9/96 <br /> Instrument I D #: GCHP5 <br /> Cone Spiked. 1000pg/L <br /> LCS Result 990 <br /> LCS %Recov 99 <br /> IVIS/MSD 50-150 <br /> LCS 60-140 <br /> Control Limits <br /> *Spike diluted out <br /> Please Note <br /> The LCS 1s a control sample of known,Interferent4ree matrix that Is analyzed using the same reagents, <br /> 1ject <br /> LNALY"TICAL preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> anager " MS-Matrix Spike,MSD=MS Duplicate,RPD=Relative%Difference 96111-198131-A .45> <br />