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Q� Sequoia <br />Analytical <br />1680 Rogers Avenue <br />San Jose, CA 95112 <br />Protect Shell(1) <br />Project Number Shell 620 W Charter Way, Stockton <br />'rotect Manacer Fran Thee <br />1551 Industrial Road <br />San Carlos CA,94070-4q 1 1 <br />(650) 232-9600 <br />FAX (650) 232-9612 <br />Sampled 5125/99 <br />Received 5126199 <br />Reported 6/22/99 <br />Total Purgeable Hydrocarbons (C6 -C12), BTEX and MTBE by DHS LUFT/Quality Control <br />Sequoia Analytical - San Carlos <br />Date Spike Sample QC Reporting Limit Recov RPD RPD <br />Analyte Analyzed Level Result Result Units Recov Limits % Limit % Notes* <br />Matrix Spike Dun 9060088-MSDI L905530-05 <br />Purgeable Hydrocarbons as Gasoline 6/16199 250 ND 211 ug/l 600-140 844 250 16 4 <br />Surrogate a,a,a-Trifluorotoluene 01100 110 to700-130 110 <br />Sequoia Analytical - San Carlos <br />== <br />to end ofrenort for text of notes <br />Page 15 of 16 <br />