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SEQUOIARedwood680 Chesapeake Drive * <br /> ANALYTI9CAL <br /> y <br /> (415) 364-9600 • FAX (415) 364-9233 <br /> Blaine Tech Services, Inc Client Project ID Shell, 620 Charter Way Sampled May 28, 1993 <br /> 985 Timothy Drive Sample Matrix Water Received Jun 2, 1993 <br /> San Jose, CA 95133 Analysis Method EPA 5030/8015/8020 Reported Jun 9, 1993 <br /> Attention Jim Keller First Sample # 31=13207 <br /> TOTAL PURGEABLE PETROLEUM HYDROCARBONS with BTEX DISTINCTION <br /> Reporting Sample Sample Sample Sample Sample Sample <br /> Analyte Limit I.D. I D I D I D. I D I D <br /> pg/L 3F13207 3F13208 3F13209 3F13210 3F13211 3F13212 <br /> MW-7 MW-8 MW-9 MW-10 DUP TB <br /> Purgeabie <br /> Hydrocarbons 50 11,000 12,000 120,000 N D N D N D <br /> Benzene 050 140 110 3,900 N D N D N D <br /> Toluene 050 210 150 2,600 N D N D N D <br /> Ethyl Benzene 050 290 27 1,100 N D N D N D <br /> Total Xylenes 050 1,100 3,400 12,000 N D N D N D <br /> Chromatogram Pattern Gas Gas Gas - - -- <br /> Quality Control Data <br /> Report Limit Multiplication Factor 40 40 400 1 0 1 0 1 0 <br /> Date Analyzed 6/7/93 6/7/93 6/8/93 6/8/93 6/7/93 6/7/-3 <br /> Instrument Identification GCHP-3 GCHP-3 GCHP-2 GCHP-2 GCHP-3 GCHP-3 <br /> Surrogate Recovery, % 103 100 110 101 97 90 <br /> (DC Limits = 70-110%) <br /> Purgeable Hydrocarbons are quantitated against a fresh gasoline standard <br /> Analytes reported as N D were not detected above the stated reponinq limit <br /> EOUOW ANALYTICAL <br /> I <br /> Bila'da Lee i <br /> Project hd"anagir 31`13201 BLA <2> <br />