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Testing and Data Management Services Analytical Report <br /> 1 101 Richfield Road o Placentia, CA 92870 a (714) 572-3270 o Fax (714) 572-3274 <br /> CLIENT BLAINE TECH SERVICES, INC LAB RECEIVING# Ron.t 25 <br /> Q0, <br /> ATTN MR JIM KELLER <br /> WIC# 204-7524-4305 <br /> PROJECT# NONE <br /> PROJECT NAME SHELL-620 WEST CHARTER WAY, STOCKTON Prepared 8130196 <br /> MATRIX LIQUID Analyzed 8130196 <br /> Spl Prep Meth EPA 5030 P UNIT ll Analyst AR <br /> EPA 8020 Partial 18015 TPH-Modified Gasoline " %Surrogate Recovery <br /> Client Ethyl Total TPH BTEX TPH <br /> Lab ID Sample ID D F Benzene Toluene Benzene Xylene Gasoline 80-120 80-120 <br /> RA083096 METHOD BLANK 1 ND ND NO ND NO 103 97 <br /> AA79598 MW-1 1 NO ND NO ND NO 109 100 <br /> AA79599 MW-2 20 1200 250 1200 4500 58000 105 109 <br /> AA79600 MW-3 1 NO ND NO NO NO 110 103 <br /> AA79601 MW-4 1 74 37 20 45 1500 120 118 <br /> AA79602 MW-5 1 0 7 ND NO ND ND 108 102 <br /> AA79603 MW-6 1 NO ND ND NO NO 108 101 <br /> AA79604 MW-7 1 37 75 23 37 1300 111 105 <br /> AA79605 MW-8 1 1 5 1 5 NO 0 8 85 101 107 <br /> AA79606 MW-9 50 1600 250 1500 3900 44000 100 103 <br /> AA79607 MW-10 1 NO NO 08 2 3 87 98 95 <br /> 79608 DUP 1 75 36 21 50 1900 119 123- <br /> 79609 EB 1 ND ND NO ND JND 111 104 <br /> Limit Of Quantitation (LOQ) 0 5 0 5 05 0 5 50 <br /> Method Detection Limit(MDL) 01 01 01 0 2 50 <br /> NOTES <br /> ND denotes Not Detected at the indicated Limit Of Quantitation(LOQ) <br /> Sample detection limits can be determined by multiplying the sample Dilution Factor(D F) by the Method Detection Limit(MDL) <br /> "Excluding MTBE concentration <br /> *"Out of criteria due to coeluban of analytes with the surrogate <br /> QUALITY CONTROL DATA , EPA - 8020Part /8095Mod. <br /> ACCURACY PRECISION <br /> LABORATORY CONTROL SPIKE LCS %LCS LCSD %LCSD ACP ACP <br /> STANDARD/DUPLICATE CONC ll II 11 %LCS RPD %RPD <br /> Benzene 80 81 101 82 103 80-120 1 0-25 <br /> Toluene 80 83 104 85 106 80-120 2 0-25 <br /> Ethyl Benzene 8 0 82 103 84 105 80-120 2 0-25 <br /> AUDIT DATA LAB ID BATCH # QC STD# ANALYZED <br /> LABORATORY CONTROL STANDARD(LCS) IBT083096 GC310 18130196 <br /> ACCURACY PRECISION <br /> MATRIX SPIKE/ SPIKE MS %MS MSD %MSD ACP ACP <br /> MATRIX SPIKE DUPLICATE CONC it 11 l %MS RPD % RPD <br /> Benzene 80 71 89 71 89 80-120 0 0-25 <br /> Toluene 80 73 91 73 91 80-120 0 0-25 <br /> AIIIIIIIIIkEthyl Benzene 80 71 89 72 90 80-120 1 0-25 <br /> AUDIT DATA LAB ID SAMPLE ID BATCH # QC-STD# ANALYZED <br /> AA79609 I EB IBT083096 GC275 8130196 <br /> This report is preceded by a cover sheet that contains vital Information <br /> Approved by the State al Cadonlia DePtshnent c(Heolth Services&A2LA-ArTwtwM AssoU rcn far Lcoctatary A00adnatlon <br /> This report is suornmed far hhe ciwd to whore tr!addressed ArN reproouc%n or use of the LaborafarV s awns to adverttslrsg cr PL06C"Y Vats A auihCrUa`cn is P ctslottea <br /> htse crakltec4 resets vANn tt"report relate aW to to specft comomnds and sarnofes krvestttaatea and mrN not necessa*reflect other apparentN stmsor morenoi from the some ar a smlla facatlon <br />