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UOC ANALYTICAL, GLENDALE QC REPORT109802259 PAaE t DATE PRINT 23 FEB 1998 AQUEOUS SAMPLES ------ METHOD BLANK ------ --------------- LAB CONTROL -------------- ---------------- MATRIX QC ---------------- LCS LCSD RPD RPD MS MSD RPD RPD UNITS RESULT PQL FLG %REC FLG %REC FLG LCL UCL RPD UCL FLG %REC FLG %REC FLG LCL UCL RPD UCL FLG Batch GAS*989019 Method 8020A - Aromatic Volatile Organics, con't m- and p-Xylene Isomers ug/L 0 26 10 - 101 - 107 - 74 118 6 - - 81 - 81 - 72 117 0 25 - o-Xylene ug/L 0 5 - 100 - 104 - 74 118 5 - - 87 - 87 - 72 117 0 25 - [a,a,a-Trifluorotoluene] Percent 98 - - 99 - 99 - 76 126 - - - 105 - 105 - 76 126 - - - I Batch GAS*989021 Method 8015M - Modified 8015 TPN (Gasoline Range) ug/L 0 300 - 94 - 87 - 80 124 7 - - 84 - 85 - 71 130 1 25 - [a,a,a-Trifluorotoluene] Percent 93 - - 92 - 98 - 76 126 - - - 104 - 105 _ 76 126 - - - Batch GAS*989021 Method 8020A - Aromatic Volatile Organics Benzene ug/L 0 5 - 96 - 114 - 76 155 17 - - 108 - 107 - 70 153 1 25 - Toluene ug/L 0 5 - 97 - 114 - 76 122 16 - - 89 - 89 - 70 124 0 25 - Ethylbenzene ug/L 0 5 - 96 - 112 - 76 119 15 - - I04 - 103 - 71 119 1 25 - Methyl-tert-butylether ug/L 0 30 - 95 - 113 - 58 147 18 - - - NC - NC - - - - PJC Total Xylene isomers ug/L 0 20 - 98 - 113 - 74 118 15 - - 97 - 97 - 72 117 0 25 m- and p-Xylene Isomers ug/L 0 10 - 98 - 113 - 74 118 14 - - 86 - 86 - 72 117 0 25 - o-Xylene ug/L 0 5 - 97 - 113 - 74 118 15 - - 95 - 95 - 72 117 0 25 - [a,a,a-Trifluorotoluene] Percent 93 - - 92 - 98 - 76 126 - - - 104 - 105 - 76 126 - - - Batch GAS*989022 Method 8015M - Modified 8015 TPH (Gasoline Range) ug/L 0 300 - 95 - 85 - 80 124 11 - - 73 - 73 - 71 130 0 25 - [a,a,a-Trifluorotoluene] Percent 99 - - 99 - 98 - 76 126 - - - 106 - 119 - 76 126 - - - Batch GAS*989022 Method 8020A - Aromatic Volatile Organics Benzene ug/L 0 5 - 102 - 102 - 76 155 0 - - 99 - 101 - 70 153 1 25 - Toluene ug/L 0 5 - 103 - 103 - 76 122 1 - - 86 - 85 - 70 124 1 25 - Ethylbenzene ug/L 0 5 - 104 - 102 - 76 119 2 - - 103 - 102 - 71 119 1 25 - Methyl-tert-butylether ug/L 0 30 - 96 - 102 - 58 147 6 - - 99 - 109 - 53 177 10 30 - Total Xylene Isomers ug/L 0 20 - 105 - 103 - 74 118 2 - - 87 - 84 - 72 117 3 25 - m- and p-Xylene Isomers ug/L 0 10 - 106 - 104 74 118 2 - - 84 - 82 - 72 117 2 25 o-Xylene ug/L 0 5 - 105 - 102 - 74 118 3 - - 92 - 89 - 72 117 4 25 [a,a,a-Trifluorotoluene] Percent 99 - - 99 - 98 - 76 126 - - - 106 - 119 - 76 126 - - -