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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (650) 364-9600 FAX(650)364-9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988-960o FAX(510)988-%73 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921-9600 FAX(916)921-0100 <br /> Blaine Tech Services- Client Proj ID Shell Stockton/971117-M1 Sampled 11/17/97 <br /> 1680 Rogers Avenue Sample Descript MW-3 Received 11/26/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 12/01/97 <br /> Attention Fran Thie Lab Number 9711F35-03 Reported 12111197 <br /> QC Batch Number MS120197MTBEH6A <br /> Instrument ID H6 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> mg/L mg/L <br /> Ethanol 050 N D <br /> t-Butanol 010 N D <br /> Methyl t-Butyl Ether (MTBE) 00020 00072 <br /> Di-Isopropyl Ether (DIPE) 00020 N D <br /> Ethyl t-Butyl Ether(ETBE) 00020 N D <br /> t-Amyl Methyl Ether (TAME) 00020 N D <br /> Surrogates Control Limits% % Recovery <br /> 1,2-Dichloroethane-d4 76 114 100 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQUOI ICAL - ELAP #1210 <br /> 7 <br /> y Pen r <br /> Project Manager Page 7 <br />