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K!ANffVAALYTICAL <br /> Report Number : 11203 <br /> Date : 03/03/98 <br /> LLC <br /> - Project Name : K&S Gas and Grocery <br /> Project Number : 98-0225-20-1 <br /> Sample : P-3 Matrix : Soil <br /> Sample Date :02/20/98 <br /> Method <br /> Measured Reporting Analysis Date <br /> Parameter Value Limit Units Method Analyzed <br /> Methyl-t-butyl ether (MTBE) 0.10 0.020 mg/Kg EPA 8260B 03/02/98 <br /> Diisopropyl ether (DIPE) < 0.020 0.020 mg/Kg EPA 8260B 03/02/98 <br /> Ethyl-t-butyl ether (ETBE) < 0.020 0.020 mg/Kg EPA 8260B 03/02/98 <br /> Tert-amyl methyl ether (TAME) < 0.020 0.020 mg/Kg EPA 8260B 03/02/98 <br /> Tert-Butanol 0.51 0.020 mg/Kg EPA 8260B 03/02/98 <br /> Dibromofluoromethane (Surr) 81.3 % Recovery EPA 8260B 03/02/98 <br /> Toluene - d8 (Surr) 91.2 % Recovery EPA 8260B 03/02/98 <br /> Sample : P-4 Matrix : Soil <br /> Sample Date :02/20/98 <br /> Method <br /> Measured Reporting Analysis Date <br /> Parameter Value Limit Units Method Analyzed <br /> - Methyl-t-butyl ether (MTBE) 0.019 0.0050 mg/Kg EPA 8260B 03/02/98 <br /> Diisopropyl ether (DIPE) < 0.0050 0.0050 mg/Kg EPA 8260B 03/02/98 <br /> Ethyl-t-butyl ether (ETBE) < 0.0050 0.0050 mg/Kg EPA 8260B 03/02/98 <br /> Tert-amyl methyl ether (TAME) < 0.0050 0.0050 mg/Kg EPA 8260B 03/02/98 <br /> Tert-Butanol 0.13 0.0050 mg/Kg EPA 8260B 03/02/98 <br /> m Dibromofluoromethane (Surr) 97.8 % Recovery EPA 8260B 03/02/98 <br /> Toluene- d8 (Surr) 93.9 % Recovery EPA 8260B 03/02/98 <br /> Approved By: Jo I Kiff <br /> 720 Olive Drive, Suite D Davis, CA 95616 916-297-48 <br />