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r <br /> I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> lie <br /> campFA40 McCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ft//www mcbell co m E-mail masn@mccampbell com <br /> rAdvanced GeoEnvironmental Client Project ID K& S Gas&Grocery Date Sampled 12/19/00 <br /> r <br /> Date Received 12/20/00 <br /> 4005 North Wilson Way <br /> Stockton, CA 95205 Client Contact Calvin Lee Date Extracted 12123-12/26/00 <br /> r Client P O Date Analyzed 12/23-12/26/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> rLab ID 56444 56445 56446 <br /> Client ID <br /> MW1/ MW2/ MW3/ Reporting Limit <br /> 12-19-00 12-19-00 12-19-00 <br /> r --- <br /> Matrix � - - W -=W— - W S w <br /> Compound Concentration* ug/kg ug/L <br /> rDi-isopropyl Ether(DIPE) ND<63 ND<85 ND<25 S 0 1 0 <br /> rEthyl tert-Butyl Ether(ETBE) ND<63 ND<85 ND<25 50 1 0 <br /> lieMethyl-tent Butyl Ether(MTBE) 670 1.r 110 54 50 10 <br /> tert-Amy]Methyl Ether(TAME) ND<63 ND<85 ND<25 so 1 0 <br /> tert-Butanol ND<320 ND<430 ND<130 25 50 <br /> rMethanol ND<13,000 ND<17,000 ND<5000 1000 200 <br /> Ethanol ND<3200 s ND<4300 ND<1300y - 250 50 - <br /> Surrogate Recoveries(%) <br /> Dibromot3uoromethane 102 104 97 <br /> Comments h <br /> water samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> r <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> r <br />