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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H2100803 Date 10/15/2002 Page 5 <br /> Project Name DARPETRO#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No NA Method 8260FA <br />' Prep Meth SW5030B <br /> Field ID MW-3 Lab Samp ID 5130-2W <br />' Descr/Location MW-3 Recd Date 10/08/2002 <br /> Sample Date 10/07/2002 Prep Date 10/09/2002 <br /> Sample Time 1420 Analysts Date 10/09/2002 <br />' <br /> Matrix Water QC Batch VWMS-0092 <br /> Basis Not Filtered Notes <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) Z89 50 MRL 85 UG/L 10 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UG/L 1 <br />' tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MRL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL 1 7Q UG/L 1 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 70-130 SLSA 100% <br /> 1,2-Dirhloroethane-d4 70-130 SLSA 742% <br /> I <br /> 1 <br /> t <br /> t <br /> Approved by Date <br />