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Castle Analytical Laboratory, Atwater, CA <br /> ILab Report No H2100803 Date 10/15/2002 Page 4 <br /> Project Name DARPETRO#8 Analysis Volatile Organic Compounds by GCIMS Fuel <br /> Project No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-13 Lab Samp ID 5130-10W <br /> Descr/Location MW-13 Rec'd Date 10/08/2002 <br /> Sample Date 10/07/2002 Prep Date 10/09/2002 <br /> Sample Time 1130 Analysis Date 10/09/2002 <br /> Matrix Water OC Batch VWMS-0092 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0 289 05 MRL NO UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL NO UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0 067 05 MRL NO UG/L 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MRL NO UG/L 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL NO UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 70-130 SLSA 966% <br /> 1,2-Dichloroethane-d4 70-130 SLSA 836% <br /> I <br /> Approved by _ __.__ Date <br /> I <br />