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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798 1620 Fax 925-7981622 � <br /> Websue www mccanipbell com E mail mamQmecampbell com <br /> ICastle Analytical Laboratory Chent Project ID #8367/Beneto#8 Date Sampled 07/21/05 <br /> 2333 Shuttle Drive Bldg 9081909 <br /> Date Received 07/22/05 <br /> IAtwater, CA 95301 Client Contact James Phillips Date Extracted 07/25/05 <br /> Client P O Date Analyzed 07/25/05 <br />' Oxygenated Volatile Organics f EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0507366 <br />' Lab ID 0507366-004A i 0507366-005A —0507366-006A 0507366-007A <br /> I � <br /> Client lD ---B--4-72-0---- B-4 92 0 I B-4 120 0 B-4 143 0 Reporting Limit for <br /> Matrix W _TW----- W �T W ----- DF=1 <br /> DF 10 W <br /> i <br /> fCompound Concentration uglkg pg/L <br /> tert-Amyl methyl ether(TAME) ND<5 0 ND ND ND NA 05 <br /> i <br />' t-Butyl alcohol(TBA) i ND<50 13 ND ND NA 50 <br /> 1 2 Dibromoethane(EDB) ND<5 0 I ND ND ND NA 0 5 <br /> i <br /> I1,2-Dichloroethane(1 2-DCA) i ND<5 0 ND 1 1 087 NA 05 <br /> Disopropyl ether(DIPE) ND<5 0 C 055 I 086 — ND - NA— 0 5 <br /> lie <br /> —a ------i- — ----T - — - <br /> Ethanol ND<500 ND ND + ND NA 50 <br />' Ethyl tert-butyl ether(ETRE) -- ND<5 0 ND I ND ND NA 0 5 <br /> t <br /> Methanol ND<5000 } ND ND ND NA 500 <br />' Methyl-t butyl ether(MTBE) ND<5 0 j 23 I ND T ND — NA 0 5 <br />' Surrogate Recoveries(%) <br /> */aSSI 108 ! 116 109 101 <br /> ' I <br /> water and vapor samples are reported toµg/L sod/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and 11 TCLP&SPLP <br /> extracts are reported in mg/L wipe samples to pg/wipe <br />' ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or coelutes with another peak,&)low surrogate due to matrix interference <br />' h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than--1 vol %sediment,3)sample diluted due to high <br /> organic content/matnx interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> re orttn limit raised due to insufficient sam le amount,n results are reported on a dry weight basis, see attached narrative <br /> I <br /> �I <br /> IDHS Certification No 1644 _ , Angela Rydelius, Lab Manager <br />