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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No . H5011201 Date 01/21/2005 Page 1 <br /> Protect Name BENETO TANK LINES#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-1 Lab Samp ID 7715-1 W <br /> Descr/Location MW-1 Recd Date 01/12/2005 <br /> Sample Date 01/11/2005 Prep Date 01/19/2005 <br /> Sample Time 1632 Analysis Date 01/19/2005 <br /> Matrix Water QC Batch VWMS-1195 <br /> Basis Not Filtered Notes DF <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 145 25 MRL 30Q UG/L 50 <br />' Ethyl tert-butyl ether(ETBE) 420 25 MRL ND UG/L 50 <br /> tert-Amyl methyl ether(TAME) 335 25 MRL ND UG/L 50 <br /> Di-isopropyl ether(DIPE) 775 25 MRL ND UG/L 50 <br />' tert-Butyl alcohol (TBA) 440 1000 MRL ND UG/L 50 <br /> 1,2-Dichloroethane 405 25 MRL ND UG/L 50 <br /> 1,2-Dibromoethane 460 25 MRL ND UG/L 50 <br />' SURROGATE AND INTERNAL, STANDARD RECOVERIES <br /> Toluene-d8 63-132 SLSA 937% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 859% 1 <br />' DF Reporting limits elevated due to matrix interferences <br /> I <br /> i <br /> Approved by �'� Date <br />