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ICastle Analytical Laboratory, Atwater, CA <br /> Lab Report No H5011201 Date 01/21/2005 Page 12 <br /> Project Name BENETO TANK LINES#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br /> I Project No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-8 Lab Samp ID 7715-8W <br /> Descr/Location MW-8 Recd Date 01/12/2005 <br /> Sample Date 01/11/2005 Prep Date 01/19/2005 <br /> Sample Time 1104 Analysis Date 01/19/2005 <br /> Matrix Water OC Batch VWMS-1195 <br /> Basis Not Filtered Notes OF <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0 578 1 MRL 41 UGIL 2 <br />' Ethyl tent-butyl ether(ETRE) 0168 1 MRL NO UGIL 2 <br /> tert-Amyl methyl ether(TAME) 0134 1 MRL NO UGIL 2 <br /> Di-isopropyl ether(DIPE) 0 310 1 MRL ND UGIL 2 <br />' tert-Butyl alcohol {TBA} 176 40 MRL 45. UGIL 2 <br /> 1,2-Dichloroethane 0162 1 MRL ND UGIL 2 <br /> 1,2-Dibromoethane 1 0184 1 MRL NO UGIL 2 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 63-132 SLSA 100% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 949% 1 <br />' DF Reporting limits elevated due to matrix interferences <br /> I <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> • <br /> 1 <br /> Approved by Date ` <br />