|
MINIMUM VERIFICATION LABORATORY ANALYSIS
<br />All analysis methods are the designated EPA methods described W EPA SW 846, Third Mtion. Those McLnoas not iouuu iat byy o-tv ill t;
<br />specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix D (B), Table 3-5 on page A20 for minimum detection
<br />limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri -Regional Board Staff Recommendations for Initial Evaluation and
<br />Investigation of UST's" for the waste and motor oil minimum detection Gmuts. Detection Limits that remain below the MCL, STLC or
<br />Allowable Limit pf the contaminant in question will be accepted, however laboratory shall utilize the most eonservztive method.
<br />LABORATORY ANALYSES TERN11NOLOGY:
<br />TPH-G Total Petroleum Hydrocarbon, Gasoline, GC/FI D (5030) 8015 mod or GC/MS 8260
<br />TPH-D Total Petroleum Hydrocarbon, piesel, GC/FID (3550), 8015 mod or GC/MS 8260
<br />BTX & EBenzene, Toluene, Xylene & Ethyl Semene, GGPID 8020 or GC/MS 8260
<br />CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240 or 8260
<br />TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />OXY08NATES MTBE, ETRE, TAME, DIPS, & TBA GUMS 8260 (For MTEE screen only you may use 8020)
<br />METALS ICAP or AA Inductively Couplcd Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000, Metals:
<br />CAdmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />PCB Polychlorinated Biphenyls, GC/MS 8270 or 8090
<br />GC -FID Gas Chromatography, Flame Ionization Detection
<br />Method 3050 Acid digestion
<br />N4cthod 3540 Soxhlet sample preparation
<br />Method 3550 Sonication sample preparation, extraction method
<br />Mcthod 5030 Purge and trap sample preparation
<br />QA/QC Quality Assurance/Quality Control
<br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns are preferred to packed columns, a
<br />packed column may be used as a "first cut" with "dirty" samples or once the hydro=bons have been characterized and proper QA/QC is followed_ For
<br />drinking water sources, EPA recommends that the 500 series for volatile organic should be used in prefercnee to the 600 series because the detection
<br />limits are lower and the QA/QC is better_ Samples exhibiting any level of heavy metal cont3TrAnation may require further analysis. PHS-EHD
<br />recommends holding those samples until disposal is indicated.
<br />FH 23 046 (Revised 05/09/00)
<br />OXYGEN
<br />TANK
<br />"TANK
<br />TPH-G
<br />TPH-D
<br />STX & E
<br />CL HC
<br />TOTAL
<br />MTBE
<br />ATES
<br />ytETA;t,
<br />l'C13
<br />#
<br />CONTENTS
<br />8015
<br />8015
<br />8020
<br />8010
<br />LEAD
<br />8020
<br />(rib.
<br />IC:AP/
<br />8260
<br />8260
<br />8260
<br />8240
<br />7420
<br />8260
<br />TBApIPE.
<br />AES or
<br />8080
<br />8260
<br />7421
<br />TAME)
<br />AA
<br />8260
<br />LEADED GAS
<br />X
<br />X
<br />X
<br />X
<br />UNI. GAS
<br />X
<br />x
<br />X
<br />DIESEL
<br />X
<br />X
<br />KEROSENE
<br />X
<br />X
<br />X
<br />UNTO FUEL
<br />X
<br />X
<br />X
<br />X
<br />X
<br />PROD. OIL
<br />X
<br />X
<br />X
<br />CHLOR.
<br />X
<br />SOLVENTS
<br />X
<br />X
<br />NONCHLOR
<br />X
<br />SOLVENTS
<br />X
<br />X
<br />WASTE\
<br />,
<br />USED OIL
<br />X
<br />X
<br />X
<br />X
<br />X
<br />X
<br />X
<br />All analysis methods are the designated EPA methods described W EPA SW 846, Third Mtion. Those McLnoas not iouuu iat byy o-tv ill t;
<br />specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix D (B), Table 3-5 on page A20 for minimum detection
<br />limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri -Regional Board Staff Recommendations for Initial Evaluation and
<br />Investigation of UST's" for the waste and motor oil minimum detection Gmuts. Detection Limits that remain below the MCL, STLC or
<br />Allowable Limit pf the contaminant in question will be accepted, however laboratory shall utilize the most eonservztive method.
<br />LABORATORY ANALYSES TERN11NOLOGY:
<br />TPH-G Total Petroleum Hydrocarbon, Gasoline, GC/FI D (5030) 8015 mod or GC/MS 8260
<br />TPH-D Total Petroleum Hydrocarbon, piesel, GC/FID (3550), 8015 mod or GC/MS 8260
<br />BTX & EBenzene, Toluene, Xylene & Ethyl Semene, GGPID 8020 or GC/MS 8260
<br />CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240 or 8260
<br />TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />OXY08NATES MTBE, ETRE, TAME, DIPS, & TBA GUMS 8260 (For MTEE screen only you may use 8020)
<br />METALS ICAP or AA Inductively Couplcd Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000, Metals:
<br />CAdmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />PCB Polychlorinated Biphenyls, GC/MS 8270 or 8090
<br />GC -FID Gas Chromatography, Flame Ionization Detection
<br />Method 3050 Acid digestion
<br />N4cthod 3540 Soxhlet sample preparation
<br />Method 3550 Sonication sample preparation, extraction method
<br />Mcthod 5030 Purge and trap sample preparation
<br />QA/QC Quality Assurance/Quality Control
<br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns are preferred to packed columns, a
<br />packed column may be used as a "first cut" with "dirty" samples or once the hydro=bons have been characterized and proper QA/QC is followed_ For
<br />drinking water sources, EPA recommends that the 500 series for volatile organic should be used in prefercnee to the 600 series because the detection
<br />limits are lower and the QA/QC is better_ Samples exhibiting any level of heavy metal cont3TrAnation may require further analysis. PHS-EHD
<br />recommends holding those samples until disposal is indicated.
<br />FH 23 046 (Revised 05/09/00)
<br />
|