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STLE ANALYTICAL LABORATORY <br /> Environmental Testing Services P O Box 1360 Winton, CA 95388 Phone (209) 384-2930 <br /> Certificate No 2079 Fax (209} 384-1507 <br />' Krazan & Associates, Inc Client Project ID 014-95262 Method 418 1 M <br /> 215 West Dakota Avenue Reference Number 534 Instrument ID IR SPEC-1 <br /> Fresno, CA 93612 Matrix Soil Prepared 9-27-95 <br /> Attn Bruce Myers Analyst Clan J Cone Analyzed 9-27-95 <br /> Reported 9-27-95 <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE PETROLEUM HYDROCARBONS <br /> t Spike Concentration 50 <br /> 'hits mg/kg <br /> LCS Batch # TRPH-9275 <br /> 0% Recovery 90% <br /> 11ontrol Limits 60-130 % <br /> ASIMSD Hatch # TRPH-9275 <br /> �AS % Recovery 86% <br /> SD % Recovery 118% <br /> ,relative % Difference 289% <br /> ' ease Note <br /> The LCS (Laboratory Check Sample) is a control sample of known, interferent free matrix that is fortified with representative analytes and <br /> nelyzed using the same reagents, preparation and analytical methods employed for the samples The LCS % recovery is used for validation <br /> F sample batch results Due to matrix effects the O.C.limits and recoveries for MSIMSD s are advisory only and are not used to accept or <br /> eject batch results <br /> ANALYST APPROVED BY <br /> Clary J Cone mes C PhrIG s <br /> Environmental Lab Director <br />